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Record W1990235323 · doi:10.1021/jp0665224

Origins of the High Thermal Stability of Alkylidene Groups on the Surface of β-Mo<sub>2</sub>C

2007· article· en· W1990235323 on OpenAlexaff
Hicham Oudghiri Hassani, Mohamed Siaj, Peter H. McBreen

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2007
Typearticle
Languageen
FieldEngineering
TopicCatalysis and Hydrodesulfurization Studies
Canadian institutionsUniversité Laval
Fundersnot available
KeywordsBond cleavageCarbideChemistryReactivity (psychology)Thermal stabilitySurface modificationCarbon fibersDesorptionCarbyneThermal desorptionInertDissociation (chemistry)OxygenChemical engineeringAdsorptionMaterials sciencePhysical chemistryOrganic chemistryCatalysisComposite materialComposite number

Abstract

fetched live from OpenAlex

Surface alkylidenes can be formed on β-Mo 2 C through the selective carbonyl bond scission of ketones and aldehydes. Spectroscopic studies show that alkylidene groups remain intact on the carbide surface to above 900 K under ultrahigh vacuum conditions. A rationalization for the anomalously high thermal stability is presented on the basis of surface analysis studies. It is shown that the relatively high reactivity of the clean carbide surface permits both carbonyl bond scission and other less selective processes involving CC and CH bond cleavage. The combined decomposition channels lead to the deposition of excess carbon and high-coordination oxygen, resulting in an inert surface on which alkylidenes are thermally stable. Removal of surface carbon, through CO desorption and carbon diffusion, occurs at high temperatures leading to a newly reactive surface. Alkylidenes trapped at low temperatures on the intrinsically passivated surface can survive until the clean surface is partially restored at high temperatures.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.025
Threshold uncertainty score0.224

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.208
Teacher spread0.199 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations9
Published2007
Admission routes1
Has abstractyes

Explore more

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