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Record W1994785186 · doi:10.1021/ja9942585

Temperature Dependence of Fusion and Fragmentation Kinetics of Triton X-100 Micelles

2000· article· en· W1994785186 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueJournal of the American Chemical Society · 2000
Typearticle
Languageen
FieldEngineering
TopicField-Flow Fractionation Techniques
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsChemistryKineticsMicelleFragmentation (computing)FusionTriton X-100Physical chemistryPulmonary surfactantBiochemistryAqueous solution

Abstract

fetched live from OpenAlex

This paper describes micelle exchange kinetics as a function of temperature for a pyrene derivative 1, a triglyceride containing a pyrenebutyrate ester, solubilized in aqueous micelles of Triton X-100. The kinetics were followed by stopped-flow fluorescence time-scan measurements in which the disappearance of excimer over time was monitored. Two components of the exchange process could be separated: a first-order process with an activation energy of 110 kJ/mol, and a second process with an activation energy of 160 kJ/mol. Because the second-order process had a rate ( k 2 ≈ 1 × 10 6 M - 1 s - 1 ) at 24.6 °C that was nearly independent of the pyrene probe ( 1, 1-octylpyrene, 1-dodecylpyrene), the second-order process was assigned to a fusion-fragmentation mechanism, rather than a “sticky-collision” mechanism. The rates of the first-order process ( k 1 ≈ 12 s - 1 for 1 ) at 24.6 °C increased with decreasing size of the probe. This step was attributed to a fragmentation-growth mechanism in which the fragmentation rate is rate limiting. Exchange by this mechanism must involve fragmentation of a micelle containing two probe molecules to form two sub-micelles large enough to bear one of the probes.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.010
Threshold uncertainty score0.173

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.004
GPT teacher head0.227
Teacher spread0.222 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it