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Record W1996572648 · doi:10.1021/jp904014u

Chelating the Surface of Zinc in Zinc Oxide Nanocrystals: Spectroscopic Characterization of ZnO Surface-Bound Eriochrome Black T and 8-Hydroxyquinoline

2009· article· en· W1996572648 on OpenAlexaff
D. Scott Bohle, Carla J. Spina

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2009
Typearticle
Languageen
FieldMaterials Science
TopicZnO doping and properties
Canadian institutionsMcGill University
Fundersnot available
KeywordsZincEriochrome Black T8-HydroxyquinolineQuenching (fluorescence)X-ray photoelectron spectroscopyAbsorption (acoustics)NanocrystalInorganic chemistryChelationMaterials scienceAbsorption spectroscopyChemistrySpectroscopyOxideAnalytical Chemistry (journal)FluorescenceAdsorptionNuclear chemistryPhysical chemistryChemical engineeringNanotechnologyMetallurgyOrganic chemistryOptics

Abstract

fetched live from OpenAlex

The surface binding of eriochrome black T (ErT) and 8-hydroxyquinoline (HQ) with zinc oxide nanocrystals is studied with UV−vis absorption and fluorescence spectroscopy. Stern−Volmer analysis of the quenching dynamics in neutral water leads to binding constants of 2.52(1) × 10 −6 and 7.14(1) × 10 −6 M −1 for the binding of HQ and ErT, respectively. ErT coordinates in a 1:1 tetrahedral geometry for about 10% of the surface zinc sites, while HQ occupies a similar coordination geometry for half of the available sites. A new transient species forms during the interaction of ErT with the zinc oxide nanocrystals which is characterized by an absorption at 680 nm.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.281

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.244
Teacher spread0.232 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations15
Published2009
Admission routes1
Has abstractyes

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