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Record W1998610472 · doi:10.1021/ja993096+

Gas-Phase Conformations of Synthetic Polymers:  Poly(ethylene glycol), Poly(propylene glycol), and Poly(tetramethylene glycol)

2000· article· en· W1998610472 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueJournal of the American Chemical Society · 2000
Typearticle
Languageen
FieldChemistry
TopicMass Spectrometry Techniques and Applications
Canadian institutionsAkzoNobel (Canada)
Fundersnot available
KeywordsChemistryEthylene glycolPolyvinyl alcoholPolymer chemistryPolymerPhase (matter)Organic chemistry

Abstract

fetched live from OpenAlex

Effects of chain flexibility and cationizing agent on the gas-phase conformations of a series of polyethers were studied. Collision cross-sections of poly(propylene glycol) (PPG) and poly(tetramethylene glycol) (PTMEG) oligomers (from the 5-mer to 14-mer) cationized by sodium were measured using ion mobility methods and compared to earlier work on sodiated poly(ethylene glycol) (PEG). Molecular mechanics/dynamics calculations show that all three polyethers form a ring of oxygen atoms around Na +, coordinating additional oxygens to the cation from above and/or below this ring. However, the number and arrangement of these oxygens are system dependent. Up to 8 oxygens in PEG coordinate Na +, but that number drops to 7 for PPG and 6 for PTMEG. The difference is attributed to changes in the structural details of the ring as well as the position of the Na + ion in that ring. Molecular mechanics/dynamics calculations were also used to investigate the structures of neutral PPG and PTMEG oligomers. In these cases, the oligomers are relatively compact below 200 K but they suddenly unfold into more extended structures between 200 and 300 K.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Insufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.072
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0040.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.264
Teacher spread0.256 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it