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Record W1999336385 · doi:10.1002/poc.708

Deconstruction of Taft's σ* parameter: QSAR meets QALE

2004· article· en· W1999336385 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueJournal of Physical Organic Chemistry · 2004
Typearticle
Languageen
FieldChemistry
TopicCrystallography and molecular interactions
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsChemistrySubstituentTaft equationLinear correlationQuantitative structure–activity relationshipAlkylLigand (biochemistry)Linear relationshipStereochemistryMedicinal chemistryComputational chemistryOrganic chemistryReceptorMathematicsStatistics

Abstract

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Abstract Taft's σ* parameter has been mostly disregarded in QSAR (quantitative structure–activity relationships) analyses because it appears to reveal only simple field‐inductive substituent effects. However, it can be shown that, when a reference reaction different from that adopted by Taft is used, the σ* values reveal considerably more subtle features. This occurs when a reference reaction parameter, p K a ′ , is used that is closely related to the Brønsted basicity of P‐donor molecules and that is regarded in QALE (quantitative analyses of ligand effects) analyses as measuring the purely σ‐donor properties of the phosphines. Values of Taft's σ* parameter for alkyl groups show an excellent linear correlation with p K a ′ but significant deviations from the correlation increase in the order CH 2 Ph (0.19)<Ph (0.46)< p ‐O‐ i ‐Pr (1.38)<OEt (1.44)<OMe (1.51)<OPh (1.82)<Cl (1.88), and the deviations for the p ‐YC 6 H 4 groups increase linearly with decreasing p K a ′ as Y changes in the order Me 2 N (0.29)<MeO (0.32)<Me (0.39)<F (0.41)<H (0.46)<Cl (0.50)<F 3 C (0.60). The new substituent effects for these ‘deviant’ groups that can be derived from the linear correlations of σ* with p K a ′ are different (even in sign for the p ‐Me 2 NC 6 H 4 group) from the original values of the Taft parameter, and they are much smaller than the additional effects detected here. These results show that σ* values contain within themselves a variety of new features that should be compared with those shown by parameters used in more recent QSAR analyses, and that might be useful in such analyses. Copyright © 2004 John Wiley & Sons, Ltd.

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Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.004
GPT teacher head0.224
Teacher spread0.220 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it