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Record W2020427372 · doi:10.1139/v01-121

Ti<sub>5</sub>Si<sub>1.3</sub>Sb<sub>1.7</sub> The first titanium silicide antimonide, forming a crystal structure not found in either binary system

2001· article· en· W2020427372 on OpenAlexfundvenueno aff
Holger Kleinke

Bibliographic record

VenueCanadian Journal of Chemistry · 2001
Typearticle
Languageen
FieldChemistry
TopicInorganic Chemistry and Materials
Canadian institutionsnot available
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsAntimonideSilicideCrystallographyCrystal structureTitaniumAntimonyChemistryTernary operationZintl phaseMetalSiliconInorganic chemistry

Abstract

fetched live from OpenAlex

Ti 5 Si x Sb 3– x can be prepared by melting mixtures of Ti, Si, and TiSb 2 . The ternary phase with x = 1.32(5) crystallizes in the W 5 Si 3 type (space group I4/mcm, Z = 8, for x = 1.32(5): a = 1034.6(2), c = 515.2(1) pm), while Ti 5 Sb 3 and Ti 5 Si 3 adopt the Yb 5 Sb 3 type and the Mn 5 Si 3 type, respectively. The Si and Sb atoms share two sites in Ti 5 Si 1.32(5) Sb 1.68 : one site is located within a linear chain with short interatomic bonds, which is almost exclusively occupied by Si (i.e., 92(1)% Si and 8% Sb), whereas the second site, being occupied by 80(2)% Sb and 20% Si, shows no significant interactions between the main group elements. Band structure calculations reveal the new silicide antimonide being metallic as a consequence of partly filled Ti d states. The structure is mainly stabilized by bonding Ti—Sb, Ti—Si, and Si—Si interactions.Key words: titanium, silicide, antimonide, crystal structure, electronic structure, structure and bonding.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0010.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.185
Teacher spread0.179 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations9
Published2001
Admission routes2
Has abstractyes

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