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Record W2021886842 · doi:10.1021/jp049406e

Reactions of One-Electron-Oxidized Methionine with Oxygen:  An ab Initio Study

2004· article· en· W2021886842 on OpenAlexaff
Mei Lan Huang, Arvi Rauk

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2004
Typearticle
Languageen
FieldChemistry
TopicFree Radicals and Antioxidants
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsChemistryRadicalPhotochemistryIntramolecular forceRadical ionOxygenMethanethiolSulfideSulfurMedicinal chemistryOrganic chemistryIon

Abstract

fetched live from OpenAlex

A one-electron oxidation of a methionine residue is thought to be a key step in the neurotoxicity of the beta amyloid peptide of Alzheimer's disease. The chemistry of the radical cation of N -formylmethioninamide ( 11 • + ) and two model systems, dimethyl sulfide ( 1 • + ) and ethyl methyl sulfide ( 6 • + ), in the presence of oxygen have been studied by B3LYP/6-31G(d) and CBS-RAD calculations. The stable form of 11 • + has a three-electron bond between the sulfur radical cation and the carbonyl oxygen atom of the i − 1 residue. The radical cation may lose a proton from the methyl or methylene groups flanking the oxidized sulfur. Both 11 • + and the resultant C-centered radicals may add oxygen to form peroxy radicals. The calculations indicate that unlike C-centered radicals the sulfur radical cation does not form a covalent bond to oxygen but rather forms a loose ion-induced dipole complex with an S−O separation of about 2.7 Å, and is bound by about 13 kJ mol -1 (on the basis of 1 • + + O 2 ). Direct intramolecular abstraction of an H atom from the α C site is unlikely. It is endothermic by more than 20 kJ mol -1 and involves a high barrier (Δ G = 79 kJ mol -1 ). The α-to-S C-centered radicals will add oxygen to form peroxy radicals. The OH BDEs of the parent hydroperoxides are in the range of 352−355 kJ mol -1, similar to SH BDEs (360 kJ mol -1 ) and α C−H BDEs (345−350 kJ mol -1 ). Thus, the peroxy radicals are oxidizing species comparable in strength to thiyl radicals and peptide backbone α C-centered radicals. Each peroxy radical can abstract a hydrogen atom from the backbone α C site of the Met residue to yield the corresponding α C-centered radical/hydroperoxide in a weakly exothermic process with modest barriers in the range of 64−92 kJ mol -1 .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.426

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.274
Teacher spread0.257 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations30
Published2004
Admission routes1
Has abstractyes

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