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Record W2021960014 · doi:10.1142/s1088424612500812

Decoupling the artificial special pair to slow down the rate of singlet energy transfer

2012· article· en· W2021960014 on OpenAlexaff
Pierre D. Harvey, Adam Langlois, Mikhail A. Filatov, Daniel Fortin, Kei Ohkubo, Shunichi Fukuzumi, Roger Guilard

Bibliographic record

VenueJournal of Porphyrins and Phthalocyanines · 2012
Typearticle
Languageen
FieldMaterials Science
TopicPorphyrin and Phthalocyanine Chemistry
Canadian institutionsUniversité de Sherbrooke
Fundersnot available
KeywordsChemistryTrimerUltrafast laser spectroscopyChromophorePorphyrinAcceptorAbsorption spectroscopyPhotochemistryFree baseSinglet stateSpectroscopyDimerCrystallographyExcited statePhysical chemistryAtomic physics

Abstract

fetched live from OpenAlex

Trimer 2, composed of a cofacial heterobismacrocycle, octamethyl-porphyrin zinc(II) and bisarylporphyrin zinc(II) held by an anthracenyl spacer, and a flanking acceptor, bisarylporphyrin free-base ( Ar = -3,5-(t Bu ) 2 C 6 H 3 ), has been studied by means of absorption spectroscopy, "steady state and time-resolved fluorescence" and fs transient absorption spectroscopy, and density functional theory (DFT) in order to assess the effect of decoupling the chromophores' low energy MOs on the rate of the singlet, S 1 , energy transfer, k ET , compared to a recently reported work on a heavily coupled trimeric system, Trimer 1, [biphenylenebis(n-nonyl)porphyrin zinc(II)]-bisarylporphyrin free-base ( Ar = -3,5-(t Bu ) 2 C 6 H 3 ). The position of the 0–0 peaks of the absorption and fluorescence spectra of Trimer 2 indicates that these porphyrin units are respectively energy donor 1, donor 2, and acceptor. The DFT computations confirm that the MOs of the cofacial donor 1-donor 2 dyad are decoupled, but significant MO coupling between donor 2 and acceptor 1 is still present despite the strong dihedral angle between their respective average planes (77.5°: geometry optimization by DFT). The fs transient absorption spectra exhibit a clear S 1 –S n fingerprint of the bisarylporphyrin zinc(II) chromophore and the kinetic trace exhibits a slow rise time of 87 ps, due to a S 1 donor 1 → donor 2 ET. The transient species donor 2 and acceptor decay respectively in the short (~1.5) ns and 6 ns time scale.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.032
Threshold uncertainty score0.668

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0020.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.240
Teacher spread0.220 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations10
Published2012
Admission routes1
Has abstractyes

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