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Record W2024685013 · doi:10.1021/ie3003446

Thermal, Oxidative, and CO<sub>2</sub>-Induced Degradation of Supported Polyethylenimine Adsorbents

2012· article· en· W2024685013 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2012
Typearticle
Languageen
FieldEngineering
TopicCarbon Dioxide Capture Technologies
Canadian institutionsUniversity of Ottawa
Fundersnot available
KeywordsPolyethylenimineAdsorptionChemical engineeringFourier transform infrared spectroscopyChemistryFlue gasDegradation (telecommunications)Thermal stabilityDesorptionMesoporous materialCarbon dioxideDiffuse reflectance infrared fourier transformMaterials scienceOrganic chemistryCatalysis

Abstract

fetched live from OpenAlex

This work examines the stability of polyethylenimine(PEI)-impregnated mesoporous silica for CO 2 removal over a wide range of conditions. The support used was a SBA-15 silica with platelet morphology and short pore channels (SBA-15PL). The effect of long-term exposure to different gaseous streams, including carbon-free air (CFair), simulated flue gas (SFG), and different CO 2 /O 2 /N 2 mixtures on the carbon dioxide adsorption capacity was investigated. Extensive CO 2 adsorption–desorption cycling using dry and humid streams at different adsorption and regeneration temperatures was also carried out. Based on adsorption data, as well as diffuse reflectance infrared Fourier transform (DRIFT) and 13 C CP MAS NMR measurements, it was found that PEI-modified adsorbents exhibit (i) high thermal stability at moderate temperatures, (ii) highly stable CO 2 uptake in the presence of moisture, (iii) extensive degradation in the presence of dry CO 2, particularly at high temperature, (iv) fast degradation upon exposure to CFair even at moderate temperatures, (v) excellent stability in the presence of humidified gases containing both CO 2 and O 2 .

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.072
GPT teacher head0.299
Teacher spread0.227 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it