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Record W2029918654 · doi:10.1021/ie020275i

Kinetics of Reaction between Hydrogen Sulfide and Sulfur Dioxide in Sulfuric Acid Solutions

2002· article· en· W2029918654 on OpenAlexafffund
Hui Wang, I. G. Dalla Lana, Karl T. Chuang

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2002
Typearticle
Languageen
FieldEngineering
TopicIndustrial Gas Emission Control
Canadian institutionsUniversity of Alberta
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsSulfuric acidChemistryHydrogen sulfideOrder of reactionInorganic chemistryReaction rateKineticsSulfur dioxideActivation energyChemical kineticsReaction rate constantSulfurSulfideCatalysisPhysical chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Our earlier study showed that when H 2 S and concentrated sulfuric acid react, H 2 S is first oxidized by molecular H 2 SO 4 and then consecutively by SO 2, a product of the first oxidation step. The rate of the first reaction was measured using initial rate analysis at temperatures and acid concentrations under which conditions the second reaction may be neglected. In this study, the kinetics of the second reaction, i.e., the reaction between hydrogen sulfide and sulfur dioxide in sulfuric acid solutions, was studied at 20−50 °C and 30−60 wt % of acid concentration, under which conditions the rate of the first reaction is negligible. The second reaction follows first-order kinetics with respect to the partial pressure of H 2 S in the gas phase and also to the concentration of SO 2 in the solution. Changes in acid concentration do not affect the rate constant. The activation energy and the preexponential factor of the reaction at all acid concentrations studied are 59.02 kJ mol -1 and 11 900 L s -1 m -2 Pa -1, respectively. Further experiments show that the measured kinetic results also apply to the second reaction in sulfuric acid at concentrations exceeding 60 wt %.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.005

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.113
GPT teacher head0.285
Teacher spread0.173 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations22
Published2002
Admission routes2
Has abstractyes

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