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Record W2034514043 · doi:10.1021/jp000810x

Density Functional Theory Analysis of Stereoelectronic Properties of Cobalamins

2000· article· en· W2034514043 on OpenAlexaff
Tadeusz Andruniów, Marek Z. Zgierski, Pawel M. Kozlowski

Bibliographic record

VenueThe Journal of Physical Chemistry B · 2000
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicPorphyrin Metabolism and Disorders
Canadian institutionsSteacie Institute for Molecular Sciences
Fundersnot available
KeywordsCorrinChemistrySteric effectsDensity functional theoryLigand (biochemistry)Bond lengthTrans effectCrystallographyStereochemistryElectronic effectIsopropylMethyl groupAlkylComputational chemistryCobaltMedicinal chemistryCrystal structureInorganic chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Density functional theory (DFT) is applied to the calculation of the steric and electronic factors which might affect the Co−C R bond activation in coenzyme B 12 . The six-coordinate cobalamins (B−[Co III (corrin)]−R, models of coenzyme B 12 ) include the actual corrin macroring as the equatorial ligand and imidazole (Im), dimethylbenzimidazole (DBI) or water (H 2 O), as the α-trans ligand (B). The β axial ligand (R) represents a series of alkyl groups with different steric bulkiness ranging from −C⋮N, −C⋮CH through methyl, ethyl, isopropyl, tert -butyl to 5‘-deoxy-5‘-adenosyl. Each trans ligand (Im, DBI or H 2 O) produces a positive correlation of the Co−C R and Co−N B bond lengths. The increasing complexity of the R group leads to two major structural correlations: a positive correlation between the Co−C R and Co−N B bond lengths and an inverse correlation between the Co−C R bond length and the flatness of the corrin ring. It is shown that stereoelectronic properties of cobalamins can only be explained on the basis of electronic considerations. Moreover, electron donation from axial ligands to the cobalt atom either by electron donating substituents or by a properly oriented external electric field caused by external electric charges is argued to be the main trigger for the activation of the Co−C R bond.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Simulation or modeling · Consensus signal: Simulation or modeling
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.011
Threshold uncertainty score0.022

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0010.001
Science and technology studies0.0010.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0040.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.204
Teacher spread0.198 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designSimulation or modeling
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations69
Published2000
Admission routes1
Has abstractyes

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