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Record W2038786358 · doi:10.1016/j.egypro.2011.01.034

Kinetics of the reaction of carbon dioxide (CO2 ) with cyclic amines using the stopped-flow technique

2011· article· en· W2038786358 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueEnergy Procedia · 2011
Typearticle
Languageen
FieldEngineering
TopicCarbon Dioxide Capture Technologies
Canadian institutionsUniversity of Regina
FundersNatural Resources CanadaNatural Sciences and Engineering Research Council of Canada
KeywordsPiperazineChemistryAmine gas treatingAqueous solutionMorpholineMedicinal chemistryReaction rateReaction mechanismKineticsZwitterionOrder of reactionChemical kineticsDiamineReaction rate constantOrganic chemistryNuclear chemistryCatalysisMolecule

Abstract

fetched live from OpenAlex

Experimentally found kinetic values (pseudo-first order rate constants) for the reaction of CO2 in different types of aqueous amines using stopped-flow technique were compared at 303.15 K. (Primary amines–1-amino-propanol(1-AP), 3-amino-propanol(3-AP),Ethylaminoethanol(EAE); Secondary amines–Ethylene diamine(EDA), 1, 3-diamino propane(DAP), 2-(amino ethyl)ethanol amine (AEEA); Cyclic amine–Piperazine; Poly amine–N-(2-aminoethyl)-1, 3-propane diamine). It was observed that polyamines and cyclic amines are having higher reaction rate than primary, and secondary amines. Therefore, the kinetics of the reaction of carbon dioxide with six cyclic amines)) in aqueous solutions has been studied at (298.15 to 313.15) K over a concentration range of (20to120) mol⋅m−3 using the stopped-flow technique.(Piperazine (PZ),1-methyl piperazine (1-MPZ),2-methyl piperazine (2-MPZ),1-ethyl piperazine (1-EPZ),N-(2-hydroxyethyl) piperazine (1-HEPZ) and 3-morpholino propyl amine (3-MOPA). PZ has the highest reaction rate and 1-MPZ has the lowest. The trend of reaction rates are given as (PZ>2-MPZ>1-EPZ>3-MOPA>HEPZ>1-MPZ). All the studied cyclic amines were found to have fractional reaction order with respect to amine varying from 0.9 to 2.43.Termolecular mechanism and Zwitterion-mechanism were used for calculating the rate parameters by fitting the experimental data.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.004
Threshold uncertainty score0.368

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.014
GPT teacher head0.184
Teacher spread0.170 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it