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Record W2038845565 · doi:10.1021/ma9020483

Effect of Hydroplasticization on Polymer Diffusion in Poly(butyl acrylate-<i>co</i>-methyl methacrylate) and Poly(2-ethylhexyl acrylate-<i>co</i>-<i>tert</i>-butyl methacrylate) Latex Films

2009· article· en· W2038845565 on OpenAlexaff
Mohsen Soleimani, Jeffrey C. Haley, Willie Lau, Mitchell A. Winnik

Bibliographic record

VenueMacromolecules · 2009
Typearticle
Languageen
FieldChemistry
TopicAdvanced Polymer Synthesis and Characterization
Canadian institutionsUniversity of Toronto
Fundersnot available
KeywordsMethacrylatePolymer chemistryMethyl methacrylateGlass transitionAcrylatePolymerPlasticizerMaterials scienceChemical engineeringDiffusionButyl acrylateCopolymer2-Hydroxyethyl MethacrylateChemistryComposite materialThermodynamics

Abstract

fetched live from OpenAlex

We compare the influence of humidity on the polymer diffusion rate in films formed from two different polymer latex samples whose polymers have the same glass transition temperature ( T g ≈ 12 °C) but different hydrophilicity: poly(butyl acrylate- co -methyl methacrylate), P(BA−MMA), and the more hydrophobic poly(2-ethylhexyl acrylate- co - tert -butyl methacrylate), P(EHA−tBMA). The diffusion process was monitored by fluorescence resonance energy transfer (FRET) at 25 °C and at 0, 23, 54, 85 and 98% relative humidities. The results show that the polymers diffused more rapidly in films aged at higher humidities, and thus were characterized by higher apparent diffusion coefficients ( D app ). By performing a master curve analysis, we obtained humidity related shift factors ( a H ). Not all the water taken up by these latex films contributes to enhance diffusion rates. Some of the water absorbed at high humidities is present in the form of water pools and microcavities (free water) and does not actively contribute to plasticization. We used FTIR spectra to obtain information about how water resides in the copolymer films. Although water is poorly miscible with most polymers, our results show that water molecules dispersed molecularly among the chains are highly efficient as a plasticizer and a promoter of polymer diffusion in latex films.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.094
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.253
Teacher spread0.248 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations34
Published2009
Admission routes1
Has abstractyes

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