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Record W2040780615 · doi:10.1117/12.659821

Amplification of the index of refraction of aqueous immersion fluids with crown ethers: a progress report

2006· article· en· W2040780615 on OpenAlexaff
Juan López‐Gejo, Joy T. Kunjappu, Nicholas J. Turro, Will Conley

Bibliographic record

VenueProceedings of SPIE, the International Society for Optical Engineering/Proceedings of SPIE · 2006
Typearticle
Languageen
FieldEngineering
TopicNanofabrication and Lithography Techniques
Canadian institutionsSemtech (Canada)
Fundersnot available
KeywordsSolubilityAqueous solutionChemistryBoiling pointRefractive indexDilutionViscosityInorganic chemistrySalt (chemistry)High-refractive-index polymerCrown etherChemical engineeringOrganic chemistryMaterials scienceThermodynamicsComposite materialIon

Abstract

fetched live from OpenAlex

There is a current need for high refractive index (RI) materials that can be used in aqueous systems for improving 193 nm immersion photolighography. Although heavy metal salts such as Ca2+ and Ba2+ have the potential to substantially increase the RI of aqueous solutions, the water solubility of these salts with common anions is often too low to achieve concentrations that significantly increase the RI to the desired values. We have therefore investigated the use of crown ethers to enhance the solubility of these cations. Most of the crown ethers are soluble in water, environmentally benign and commercial and inexpensive materials. Details of the preliminary studies on the proposed model system are presented in this paper. 15-crown-5-ether and 12-crown-4-ether are liquids at room temperature and therefore can be used as neat liquids as immersion fluids without dilution in water. Saturation of crown ethers with inorganic salts do not lead to any increase of the refractive index due to the low solubility of those in such an apolar media. Thus, the use of inorganic salt as refractive index enhancement agent does not seem to be a desirable proposition in the present case. Instead, the use of crown ethers or their derivates can be alternative system since these compounds have properties, such as density, viscosity and boiling point, similar to aqueous media.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.221
Teacher spread0.214 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2006
Admission routes1
Has abstractyes

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Same venueProceedings of SPIE, the International Society for Optical Engineering/Proceedings of SPIESame topicNanofabrication and Lithography TechniquesFrench-language works237,207