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XRD<sup>2</sup> Stress Measurement for Samples with Texture and Large Grains

2013· article· en· W2040930857 on OpenAlexaff
Bob B. He

Bibliographic record

VenueMaterials science forum · 2013
Typearticle
Languageen
FieldMaterials Science
TopicX-ray Diffraction in Crystallography
Canadian institutionsBruker (Canada)
Fundersnot available
KeywordsMaterials scienceAnisotropyDiffractionTexture (cosmology)Intensity (physics)Orientation (vector space)Grain sizeStress (linguistics)StatisticsX-ray crystallographyOpticsCondensed matter physicsAnalytical Chemistry (journal)Composite materialMathematicsPhysicsGeometryImage (mathematics)Artificial intelligenceChemistryComputer science

Abstract

fetched live from OpenAlex

Stress measurement on samples with texture and large grains is always a challenge. The diffraction peak intensity varies dramatically with different sample orientation. The macroscopic elasticity becomes anisotropic due to strong preferred orientation. The large grains may results in a big error in 2θ due to poor sampling statistics. The fitting results of the conventional sin2ψ method is extremely sensitive to texture and large grains. When stress is measured with a 2D detector, most of the above adverse effects can be minimized or eliminated. The data integration helps to smooth out rough diffraction profiles due to large grain size, texture, small sample area or weak diffraction. The large angular coverage and multiple diffraction rings can minimize the effect of the macroscopic anisotropy. The weighted least squares regression and intensity threshold can further reduce the effect of poor statistics associated with texture and large grains. Multiple {hkl} rings may be used to measure the stress to improve the statistics and minimize the elastic anisotropy effect.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.003
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.072
Threshold uncertainty score0.242

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0020.003
Meta-epidemiology (narrow)0.0020.002
Meta-epidemiology (broad)0.0020.000
Bibliometrics0.0020.004
Science and technology studies0.0010.001
Scholarly communication0.0010.002
Open science0.0020.001
Research integrity0.0010.003
Insufficient payload (model declined to judge)0.0720.019

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.241
Teacher spread0.222 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2013
Admission routes1
Has abstractyes

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