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Record W2044874267 · doi:10.1021/jp811517p

Structures of Water Molecules at the Interfaces of Aqueous Salt Solutions and Silica: Cation Effects

2009· article· en· W2044874267 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2009
Typearticle
Languageen
FieldPhysics and Astronomy
TopicSpectroscopy and Quantum Chemical Studies
Canadian institutionsUniversity of British Columbia
Fundersnot available
KeywordsSilanolAqueous solutionChemistryMoleculeInfrared spectroscopyHydrogen bondAlkali metalIonic bondingInorganic chemistryIonic radiusIonChemical physicsAnalytical Chemistry (journal)Physical chemistryOrganic chemistryCatalysis

Abstract

fetched live from OpenAlex

Structures of water molecules at water/silica interfaces, in the presence of alkali chloride, were investigated using infrared−visible sum frequency vibrational spectroscopy. Significant perturbations of the interfacial water structure were observed on silica surfaces with the NaCl concentration as low as 1 × 10 −4 M. The cations, which interact with the silica surface via electrostatic interaction, play key roles in perturbing the hydrogen-bond network of water molecules at the water/silica interface. This cation effect becomes saturated at concentrations around 10 −2 to 10 −1 M, where the sum frequency generation peaks at 3200 and 3400 cm −1 decrease by 75%. Different alkali cation species (Li +, Na +, and K + ) produce different magnitudes of perturbation, with K + > Li + > Na + . This order can be explained by considering the effective ionic radii of the hydrated cations and the electrostatic interactions between the hydrated cations and silica surfaces. The interfacial water structure associated with the 3200 cm −1 band is more vulnerable to the cation perturbation, suggesting that the more ordered water structure on silica is likely associated with the vincinal silanol groups, which create a higher local surface electrical field on silica.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.015
Threshold uncertainty score0.149

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.238
Teacher spread0.233 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it