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Record W2045226502 · doi:10.1021/je0603731

Ternary Mutual Diffusion Coefficients from Error-Function Dispersion Profiles:  Aqueous Solutions of Triton X-100 Micelles + Poly(ethylene glycol)

2007· article· en· W2045226502 on OpenAlexaff
Helga M. Halvorsen, Elzbieta Wygnal, Michael R. MacIver, Derek G. Leaist

Bibliographic record

VenueJournal of Chemical & Engineering Data · 2007
Typearticle
Languageen
FieldChemistry
TopicDiffusion Coefficients in Liquids
Canadian institutionsWestern University
Fundersnot available
KeywordsChemistryTaylor dispersionDilutionDiffusionTernary operationEthylene glycolDispersion (optics)Aqueous solutionAnalytical Chemistry (journal)MicelleThermodynamicsChromatographyPhysical chemistryOrganic chemistryOpticsPhysics

Abstract

fetched live from OpenAlex

Taylor dispersion has gained widespread popularity for measuring diffusion in liquids. The usual procedure is to inject small volumes of solution containing solute at concentration c̄ + Δ c into carrier streams of composition c̄ . Binary mutual diffusion coefficients D are evaluated from the Gaussian distribution of the dispersed solute measured at the outlet of a long capillary tube. As a result of strong dilution of the injected solute with the carrier solution, obtaining favorable signal-to-noise ratios for the measured profiles can require unacceptably large Δ c values for solutions with strongly composition-dependent diffusion coefficients or broad dispersion profiles produced by slowly diffusing solutes. For these systems, D can be reliably evaluated from error-function profiles generated by changing the solution flowing into dispersion tube from composition c̄ − (Δ c /2) to c̄ + (Δ c /2). There are no dilution factors, so Δ c can be orders of magnitude smaller than the values employed in conventional pulse-injection techniques. In the present study, the error-function dispersion technique is extended to measure coupled diffusion in three-component solutions using small Δ c initial conditions. A least-squares procedure is developed to calculate ternary mutual D ik coefficients from profiles generated by changing the solution flowing into a dispersion tube from composition c̄ 1 − (Δ c 1 /2) and c̄ 2 − (Δ c 2 /2) to c̄ 1 + (Δ c 1 /2) and c̄ 2 + (Δ c 2 /2). D ik coefficients are measured for aqueous solutions of Triton X-100 + poly(ethylene glycol) at 25 °C to study the interactions between nonionic micelles and polymers.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.002
metaresearch head score (Gemma)0.005
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.002
Threshold uncertainty score0.008

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0020.005
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0020.002
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.021
GPT teacher head0.260
Teacher spread0.239 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations5
Published2007
Admission routes1
Has abstractyes

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