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Record W2045780258 · doi:10.4319/lom.2005.3.24

Dissolved gas measurements in oceanic waters made by membrane inlet mass spectrometry

2005· article· en· W2045780258 on OpenAlexaff
Philippe D. Tortell

Bibliographic record

VenueLimnology and Oceanography Methods · 2005
Typearticle
Languageen
FieldEarth and Planetary Sciences
TopicMarine and coastal ecosystems
Canadian institutionsUniversity of British Columbia
Fundersnot available
KeywordsSeawaterTrace gasBiogeochemical cycleMass spectrometryEnvironmental scienceSubarctic climateTransectInletEnvironmental chemistryOceanographyChemistryAnalytical Chemistry (journal)Atmospheric sciencesGeologyChromatography

Abstract

fetched live from OpenAlex

A method is presented for the shipboard analysis of dissolved gases (O2, CO2, Ar, N2, H2S, dimethylsulfide) in oceanic waters using membrane inlet mass spectrometry (MIMS). Gases are extracted from seawater across a semipermeable membrane into the ion source of the mass spectrometer. The method can be used to simultaneously measure both major and trace gases in seawater samples in near real-time. In the case of DMS, low nmol L−1 detection limits can be achieved without any concentration step. Multiple calibration and method comparison exercises conducted in the subarctic Pacific Ocean show that the MIMS method provides gas measurements that are consistent with those obtained by standard techniques, with precision of replicate samples ranging from less than 1% to approximately 5% coefficient of variation (CV). To illustrate the usefulness of the MIMS approach, depth profiles are presented for O2, CO2, N2, and DMS at various coastal and open ocean stations in the subarctic Pacific. In addition to these discrete gas measurements, the MIMS system has also been used to continuously monitor gas concentrations along underway transects. High frequency gas measurements of O2, CO2, and DMS made along two coastal transects reveal a high degree of spatial and temporal variability in gas concentrations, likely resulting from the interplay of various biological, chemical, and physical forcings. The underway MIMS data provide insight into the biogeochemical controls on gas cycling in dynamic marine waters.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Methods · Consensus signal: none
Teacher disagreement score0.003
Threshold uncertainty score0.005

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.001
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.019
GPT teacher head0.256
Teacher spread0.237 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreMethods

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations178
Published2005
Admission routes1
Has abstractyes

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