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Record W2051781327 · doi:10.1021/la025719u

Apparent Molar Volumes and Heat Capacities of Various Adsorbed Additives on Polystyrene Latexes

2002· article· en· W2051781327 on OpenAlexaff
Éric Vignola, Gérald Perron, Jacques E. Desnoyers

Bibliographic record

VenueLangmuir · 2002
Typearticle
Languageen
FieldChemistry
TopicSurfactants and Colloidal Systems
Canadian institutionsInstitut National de la Recherche Scientifique
Fundersnot available
KeywordsAdsorptionChemistryIsothermal microcalorimetryAqueous solutionThermodynamicsElectrolytePolystyreneLangmuirLangmuir adsorption modelIonic bondingChemical engineeringOrganic chemistryPhysical chemistryPolymerEnthalpy

Abstract

fetched live from OpenAlex

Flow densimetry and flow microcalorimetry have been used to study the effect of electrolytes, surfactants, and alcohols on positively and negatively charged polystyrene latexes. The thermodynamic volumes and heat capacities of transfer of the latex from water to the aqueous solutions and of the additives from water to the latex dispersions were measured as a function of the additive concentration. With some systems, the adsorption isotherms were also determined. These thermodynamic properties are largely insensitive to electrostatic interactions but depend significantly on changes in hydrophobic interactions resulting from adsorption of the additive on the latex. Negligible changes in the quantities of transfer are thus observed for electrolytes, methoxyethanol, and methanol, but ionic and nonionic surfactants are adsorbed on both types of latexes. The adsorption of medium-chain-length alcohols and alkoxyethanols increases with their hydrophobic character. A simple model based on the Langmuir isotherm, the thermodynamic properties of the additives in water, and the properties of the adsorbed additives correctly predicts the general trends of the transfer functions of the additive and of the latex. However, a detailed analysis of the data indicates that the adsorption isotherm is more complex than expected from the Langmuir equation and that the thermodynamic properties of the adsorbed species depend on the extent of coverage. At high concentrations, the volumes and heat capacities of adsorbed surfactants are of the same order of magnitude as the corresponding values of the surfactants in micellar form.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.148
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.192
Teacher spread0.179 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations8
Published2002
Admission routes1
Has abstractyes

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