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Formulation, Characterization, Study of Swelling Kinetics and Network Parameters of Poly (MA-co-VA-co-AA) Terpolymeric Hydrogels with Various Concentrations of Acrylic Acid

2013· article· en· W2052450988 on OpenAlexvenueno aff
Rubab Zohra, Zafar Iqbal

Bibliographic record

VenueJournal of Research Updates in Polymer Science · 2013
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicHydrogels: synthesis, properties, applications
Canadian institutionsnot available
Fundersnot available
KeywordsSwellingSelf-healing hydrogelsAcrylic acidGravimetric analysisKineticsMaterials sciencePolymer chemistryNuclear chemistryChemical engineeringThermogravimetric analysisDiffusionChemistryPolymerComposite materialOrganic chemistryCopolymerThermodynamics

Abstract

fetched live from OpenAlex

The ter-polymeric hydrogels of vinylacetate (VA), methacrylate (MA) and acrylicacid (AA) were prepared using ethyleneglycoldimethacrylate (EGDMA) as a cross linker and benzoylperoxide (BPO) as an initiator. The effect of acrylic acid concentration on various swelling parameters was studied at different pHs (1.0, 4.0, 5.5, 7.4 and 8.0). A promising relationship was found to exist between media penetration velocity and equilibrium media content of hydrogels at all pH values for various concentration of acrylic acid. The fastest dynamic swelling was observed for the highest concentration of acrylic acid (40 mol % of AA) at pH 8.0. In the kinetic study, during the first hours, a first order kinetics (Fick Model) was observed at pH higher than the value of pKa (4.75) of acrylic acid, the hydrogels exhibiting non-Fickian diffusion mechanism. Whereas, for the acidic media pH, a second order kinetics was observed (Schott Model). Network parameters strongly support the swelling out comes. The relaxations of the ter-polymeric chain were observed after swelling at pH 8.0 via SEM pictures. Thermo gravimetric analysis and differential scanning calorimetric analysis also agree with the above conclusions. Well controlled swelling behavior, network properties, SEM out comings and thermo-gravimetric analysis support the idea to use these hydrogels for targeted drug delivery in the colon part of the digestive tract.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.036
Threshold uncertainty score0.410

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.024
GPT teacher head0.309
Teacher spread0.285 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

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Citations0
Published2013
Admission routes1
Has abstractyes

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Same venueJournal of Research Updates in Polymer ScienceSame topicHydrogels: synthesis, properties, applicationsFrench-language works237,207