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Record W2054970025 · doi:10.1021/jp030556j

Conformational Analysis of Glutathione in Aqueous Solution with Molecular Dynamics

2003· article· en· W2054970025 on OpenAlexafffund
Outi Lampela, André H. Juffer, Arvi Rauk

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2003
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicSulfur Compounds in Biology
Canadian institutionsUniversity of Calgary
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsChemistrySteric effectsCrystallographyMolecular dynamicsIntermolecular forceCovalent bondAqueous solutionGlutathioneSide chainElectrostaticsStereochemistryComputational chemistryMoleculePhysical chemistryEnzymeOrganic chemistry

Abstract

fetched live from OpenAlex

Molecular dynamics simulations over 20 ns with the Gromacs all-atom force field, coupled with cluster analyses of the trajectories, have been applied to the sixteen charge states of glutathione (GSH) in order to examine the distribution conformations in aqueous solution as a function of pH. The simulations show that GSH is very flexible and does not adopt a strongly preferred conformation at any pH. Comparison with limited conformational data deduced from NMR analyses shows little agreement. Contrary to the NMR results which found essentially equal populations of the three rotameric forms, the simulations reveal lower populations for gauche rotameric forms of the Cys and Glu side chains. In most species, the lowest populations were found for the sterically hindered gauche−gauche orientation about the C α −C β bond in both residues, except when electrostatic attraction between oppositely charged ends, unshielded by intervening water, was found to dominate. In the majority of the enzyme-bound GSH structures extracted from the Brookhaven Protein Data Bank, the bound GSH has a conformation that is either the same or similar to that free in solution. In some cases, as in the case of solid-state GSH and the oxidized form, GSSG, crystal packing and intermolecular H-bonding interactions force the GSH skeleton into a conformation that is not seen in solution. The distribution of the separation of the Cys S atom from the Glu α C−H bond was monitored over the course of the 20 ns simulations to deduce conditions under which H atom transfer may occur from the Glu α C−H bond to a thiyl radical of the Cys moiety of GSH, as has been observed experimentally.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.013
Threshold uncertainty score0.243

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.232
Teacher spread0.228 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations50
Published2003
Admission routes2
Has abstractyes

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