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Record W2055793167 · doi:10.1021/ma061630+

Self-Assembled Morphologies of a Diblock Copolymer Melt Confined in a Cylindrical Nanopore

2006· article· en· W2055793167 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueMacromolecules · 2006
Typearticle
Languageen
FieldMaterials Science
TopicBlock Copolymer Self-Assembly
Canadian institutionsSt. Francis Xavier University
Fundersnot available
KeywordsCopolymerNanoporePolymer chemistryMaterials scienceMorphology (biology)Polymer scienceChemical engineeringSelf-assemblyNanotechnologyPolymerComposite materialGeology

Abstract

fetched live from OpenAlex

We systematically investigate the microdomain morphologies that self-assemble in a diblock copolymer melt confined to a narrow cylindrical nanopore using real-space self-consistent mean-field theory. We observe, for a bulk cylinder-forming copolymer, that a variety of novel microdomain structures emerge under confinement. As the pore diameter increases, the following sequence of stable structures occurs: single cylinder, stacked disks, single helix, double helix, toroid−sphere, and helix−cylinder. We accurately locate the pore diameters where first-order phase transitions between these morphologies occur. We vary the interaction of the diblock copolymer with the pore wall from being preferential for the minority block to neutral to being preferential for the majority block and find that the sequence of structures is unchanged, for these interactions. The pitch angle of the helices and the pore diameter can be related using a simple geometrical argument. Over the range of pore diameters we examine, phases involving arrangements of multiple straight cylinders along the pore axis have significantly higher free energy than the structures mentioned above. Our results are consistent with experiments and a recent simulated annealing study.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.229
Teacher spread0.221 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it