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Record W2062731539 · doi:10.1002/jemt.10400

Physical and chemical analysis of the siliceous skeletons in six sponges of two groups (demospongiae and hexactinellida)

2003· article· en· W2062731539 on OpenAlexfundno aff
Floyd Sandford

Bibliographic record

VenueMicroscopy Research and Technique · 2003
Typearticle
Languageen
FieldBiochemistry, Genetics and Molecular Biology
TopicMarine Sponges and Natural Products
Canadian institutionsnot available
FundersMansoura UniversityCanterbury Medical Research FoundationIowa State UniversityMcGill University
KeywordsSpiculeSpongeSponge spiculeChemical compositionMineralogyAnalytical Chemistry (journal)ChemistryGeologyPaleontologyEnvironmental chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

The siliceous skeletons of six hexactinellids and demosponges were compared using a series of physical and chemical tests. The sponges were two hermit-crab sponges (Class Demospongiae, family Suberitidae), one from Scotland, Suberites domuncula, and the other, Pseudospongosorites suberitoides, from the Gulf of Mexico, and four hexactinellids, Hyalonema sp., Euplectella aspergillum, Rhabdocalyptus dawsoni, and Aphrocallistes vastus. The operating hypothesis was that differences in the amorphous hydrated silica skeletons in Demosponges and Hexactinellids might prove taxonomically useful. Physical properties studied included SEM, glass density, glass transition temperature (Tg), TG/DTA to determine water content, and FTIR spectra. Chemical determinations were made using energy dispersive X-ray fluorescence (EDXRF). Spicular skeletal material is deposited in concentric layers around the axial canal. With the exception of differences at several bands in the IR spectra, the siliceous skeletons in demosponges and hexactinellids are largely indistinguishable. Density was similar in all sponges (range 2.03-2.13 g/cc) and similar to the density of opal (SiO2 x 1.5H2O) (mean = 2.09 g/cc). IR spectra were similar, with prominent absorption bands at 460-470, 800, and 1,090-1,100 cm(-1) (due to different vibrational modes of Si-O-Si linkages) and at 1,650 and 3,450-3,560 cm(-1) (due to water). The skeletons of all six showed similar spectra to that of silica gel both before and after heating to 1,200 degrees C. Water comprised 10-14% of the skeleton by weight, slightly higher in the demosponges. Average spicule chemical composition was 85.2% SiO2, 12.3% water, and 2.5% other elements (mainly S, Al, K, Ca, and Na). The percent amounts of Si did not differ significantly between the demosponges and the hexactinellids.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.009

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.342
Teacher spread0.328 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations115
Published2003
Admission routes1
Has abstractyes

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