MétaCan
Menu
Back to cohort
Record W2070890872 · doi:10.1021/ja012596b

Periodic Trends in Indirect Nuclear Spin−Spin Coupling Tensors:  Relativistic Density Functional Calculations for Interhalogen Diatomics

2002· article· en· W2070890872 on OpenAlexaff
David L. Bryce, Roderick E. Wasylishen, Jochen Autschbach, Tom Ziegler

Bibliographic record

VenueJournal of the American Chemical Society · 2002
Typearticle
Languageen
FieldChemistry
TopicAdvanced NMR Techniques and Applications
Canadian institutionsUniversity of CalgaryUniversity of AlbertaDalhousie University
Fundersnot available
KeywordsChemistryHomonuclear moleculeHeteronuclear moleculeCoupling constantDiatomic moleculeRotational–vibrational spectroscopyHyperfine structureSpin (aerodynamics)Density functional theoryAtomic physicsRelativistic quantum chemistryComputational chemistryMoleculeQuantum mechanicsPhysicsThermodynamics

Abstract

fetched live from OpenAlex

There have been significant advances in the calculation and interpretation of indirect nuclear spin-spin coupling (J) tensors during the past few years; however, much work remains to be done, especially for molecules containing heavy atoms where relativistic effects may play an important role. Many J tensors cannot be explained based solely on a nonrelativistic Fermi-contact mechanism. In the present work, the relativistic zeroth-order regular approximation density-functional (ZORA-DFT) implementation for the calculation of J has been applied to the complete series of homonuclear and heteronuclear diatomic halogen molecules: F(2), Cl(2), Br(2), I(2), At(2), ClF, BrF, IF, ClBr, ClI, and BrI. For all of these compounds, the reduced isotropic coupling constant (K(iso)) is positive and the reduced anisotropic coupling constant (DeltaK) is negative. With the exception of molecular fluorine, the magnitudes of K(iso) and DeltaK are shown to increase linearly with the product of the atomic numbers of the coupled nuclei. ZORA-DFT calculations of J for F(2) and ClF are in excellent agreement with the results obtained from multiconfigurational self-consistent-field calculations. The relative importance of the various coupling mechanisms is approximately constant for all of the compounds, with the paramagnetic spin-orbit term being the dominant contributor to K(iso), at approximately 70-80%. Available experimental stimulated resonant Raman spectroscopy data are exploited to extract the complete J((127)I,(127)I) tensor for iodine in two rotational states. The dependence of K(iso) and DeltaK on bond length and rovibrational state is investigated by using calculated results in combination with available experimental data. In addition to providing new insights into periodic trends for J coupling tensors, this work further demonstrates the utility of the ZORA-DFT method and emphasizes the necessity of spin-orbit relativistic corrections for J calculations involving heavy nuclei.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.734
Threshold uncertainty score0.424

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.001
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.025
GPT teacher head0.284
Teacher spread0.259 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations55
Published2002
Admission routes1
Has abstractyes

Explore more

Same venueJournal of the American Chemical SocietySame topicAdvanced NMR Techniques and ApplicationsFrench-language works237,207