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Record W2080775892 · doi:10.1021/ef200823j

Corrosion-Fouling of 316 Stainless Steel and Pure Iron by Hot Oil

2011· article· en· W2080775892 on OpenAlexaff
Tyler Stephenson, Alan Kubis, Marzie Derakhshesh, Mike Hazelton, Chris Holt, Paul E. Eaton, Bruce Newman, Anne Hoff, Murray R. Gray, David Mitlin

Bibliographic record

VenueEnergy & Fuels · 2011
Typearticle
Languageen
FieldChemistry
TopicPetroleum Processing and Analysis
Canadian institutionsNational Institute for NanotechnologyUniversity of Alberta
Fundersnot available
KeywordsFoulingCorrosionMaterials scienceMetallurgyDissolutionMicroscale chemistryOxideLayer (electronics)MackinawiteIron sulfideMetalIron oxideSulfurChromiumSulfideChemical engineeringComposite materialChemistry

Abstract

fetched live from OpenAlex

We examined the fouling and corrosion that took place when 316 stainless steel and pure iron wires were electrically heated to 540–680 °C in a liquid bath of the atmospheric bottoms fraction of a crude oil. The foulant was determined to be heterogeneous, with a thick macroscale outer layer of pitch, covering a microscale sheath of coke, which was in turn both covering and interspersed with a microscale layer of iron sulfide. This foulant was observed to delaminate from the wire surface, presumably as a result of both the generation of growth stresses and the action of gas bubbles that were evolved during the fouling process. Unexpectedly but conclusively, we observed that the underlying wire surface was heavily corroded. In the case of the stainless steel, we observed a microscale chromium oxide layer that separated the foulant from the underlying metal. This layer presumably reduced the rate of metal dissolution. The degree of corrosion was much higher in the pure iron samples, where such a layer did not exist. Our hypothesis is that there is a synergy between the measured macroscopic fouling and the underlying microscopic corrosion, where the iron from the wire reacts with the sulfur in the oil to build up the thick sulfide.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.011
GPT teacher head0.210
Teacher spread0.199 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations19
Published2011
Admission routes1
Has abstractyes

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