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Record W2083912827 · doi:10.1002/pen.20500

Comparative analysis of radical‐mediated polyethylene modifications: Vinyltriethoxysilane versus mercaptopropyltriethoxysilane addition

2006· article· en· W2083912827 on OpenAlexaff
Saurav S. Sengupta, J. Scott Parent

Bibliographic record

VenuePolymer Engineering and Science · 2006
Typearticle
Languageen
FieldMaterials Science
TopicPolymer crystallization and properties
Canadian institutionsQueen's University
Fundersnot available
KeywordsVinyltriethoxysilaneCuring (chemistry)Degree of unsaturationMaterials sciencePolyethyleneSilaneSelectivityGraftingSurface modificationOrganosiliconPolymerHydrogen peroxidePolymer chemistryMoistureChemical engineeringOrganic chemistryChemistryComposite materialCatalysis

Abstract

fetched live from OpenAlex

Abstract The efficiency and selectivity of two approaches for introducing alkoxysilane functionality to polyethylene (PE) are examined along with the moisture‐curing performance of the resulting products. Although the peroxide‐initiated grafting of vinyltriethoxysilane to PE is accompanied by undesirable crosslinking, comparable silane contents can be introduced without affecting the melt viscosity through the addition of mercaptopropyltriethoxysilane (MPTES) to the unsaturation within the polymer. Rapid hydrogen atom donation by thiols underlies this unique selectivity for grafting versus molecular weight alteration, and gives rise to a remarkable tolerance of MPTES additions to phenolic antioxidants. Direct comparisons of the moisture‐curing efficiencies provided by the two functionalization techniques reveal few significant differences in crosslink yields or composition distributions. POLYM. ENG. SCI., 46:480–485, 2006. © 2006 Society of Plastics Engineers.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.085
Threshold uncertainty score0.555

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.002
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.251
Teacher spread0.229 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations14
Published2006
Admission routes1
Has abstractyes

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