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Record W2087060958 · doi:10.1021/cg0497602

Effect of Minor Components and Temperature Profiles on Polymorphism in Milk Fat

2004· article· en· W2087060958 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueCrystal Growth & Design · 2004
Typearticle
Languageen
FieldAgricultural and Biological Sciences
TopicFood Chemistry and Fat Analysis
Canadian institutionsUniversity of GuelphExxonMobil (Canada)University of Waterloo
Fundersnot available
KeywordsCrystallizationMetastabilityPolymorphism (computer science)AnhydrousPhase (matter)ChemistryCrystallographyMaterials scienceAnalytical Chemistry (journal)ChromatographyOrganic chemistryBiochemistry

Abstract

fetched live from OpenAlex

Time-resolved synchrotron X-ray diffraction techniques were used to study the effect of cooling rates and temperature on the crystallization dynamics and polymorphism of anhydrous milk fat (AMF) and milk fat triacylglycerols (MFTs). The crystallization of AMF at fast cooling rates and low final temperatures proceeded through the metastable phase α and resulted in the formation of a mixture of phases β‘ and β. Slow cooling rates and high final temperatures resulted in the formation of phase β‘ only, with no formation of phase α nor phase β. Moreover, in the absence of polar lipids, MFTs had a decreased tendency to form the α and β phases. The formation of the β phase was largely dependent on the initial amount of α phase formed. At high cooling rates and low crystallization temperatures, polar lipids may have initiated the crystallization process together with a high melting fraction of milk fat in the α phase. In time, this metastable phase transformed to the β phase. When no α phase was initially formed (high temperatures and/or slow cooling rates), no β phase was formed either. Small-angle X-ray diffraction could be used to monitor compositional variation of crystals over time, and demonstrated that minor polar lipids present in the milk fat delayed the onset of crystallization and reduced the rate of crystal growth.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.020
Threshold uncertainty score0.213

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.012
GPT teacher head0.199
Teacher spread0.187 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it