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Record W2092176791 · doi:10.1002/cjce.21896

On the interpretation of viscosity data of suspensions of asphaltene nano‐aggregates

2013· article· en· W2092176791 on OpenAlexaffvenue
Rajinder Pal, Francisco M. Vargas

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2013
Typearticle
Languageen
FieldChemistry
TopicPetroleum Processing and Analysis
Canadian institutionsUniversity of Waterloo
Fundersnot available
KeywordsAsphalteneViscosityVolume fractionSolvationThermodynamicsRelative viscosityAtomic packing factorParticle (ecology)Volume (thermodynamics)ChemistryWork (physics)Fraction (chemistry)Materials scienceChromatographyOrganic chemistryMoleculePhysicsCrystallographyGeology

Abstract

fetched live from OpenAlex

The viscous behaviour of suspensions of asphaltene nano‐aggregates is often described in terms of the Pal and Rhodes model (Pal, Rhodes, J. Rheol. 1989, 33, 1021). The model assumes particles to be spherical in shape and takes into account the solvation or hydration of particles. However, the solvation coefficient estimated from the Pal and Rhodes model for asphaltene particles is generally too high to be realistic. Furthermore, the model does not consider the packing limitations (maximum packing volume fraction) of the asphaltene particles. A large body (14 sets) of the available viscosity data for asphaltene suspensions are reinterpreted in terms of the Krieger–Dougherty model. The data analysis indicates that asphaltene nano‐aggregates are non‐spherical disk‐shaped particles with low aspect ratio (ratio of particle thickness to particles diameter). The aspect ratio depends on the nature of the asphaltene/oil system. For a given system, it increases with the increase in the temperature. Interestingly, the maximum packing volume fraction (φm) of asphaltene particles is found to be nearly constant , independent of the nature of the asphaltene/oil system and temperature. Also the values of φm predicted from the viscosity data are in reasonable agreement with the values predicted from a percolation model. Based on the analysis carried out in this work, the following model is proposed for accurate estimation and correlation of the viscosity of asphaltene suspensions: ηr = [1 − (φ/0.37)]−0.37[η], where ηr is the relative viscosity, [η] is the intrinsic viscosity and φ is the volume fraction of asphaltene particles.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.002
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.002
Threshold uncertainty score0.004

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.002
Meta-epidemiology (narrow)0.0010.000
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0020.001
Science and technology studies0.0000.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.013
GPT teacher head0.209
Teacher spread0.197 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations14
Published2013
Admission routes2
Has abstractyes

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