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Record W2092305791 · doi:10.1103/physrevb.64.094435

EPR study of<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mrow><mml:msup><mml:mrow><mml:mi mathvariant="normal">Er</mml:mi></mml:mrow><mml:mrow><mml:mn>3</mml:mn><mml:mo>+</mml:mo></mml:mrow></mml:msup></mml:mrow></mml:math>crystal-field and<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mrow><mml:msup><mml:mrow/><mml:mrow><mml:mn>165</mml:mn></mml:mrow></mml:msup></mml:mrow><mml:mrow><mml:msup><mml:mrow><mml:mi mathvariant="normal">Ho</mml:mi></mml:mrow><mml:mrow><mml:mn>3</mml:mn><mml:mo>+</mml:mo></mml:mrow></mml:msup></mml:mrow><mml:mrow><mml:msup><mml:mrow><mml:mo>−</mml:mo><mml:mi mathvariant="normal">E</mml:mi><mml:mi mathvariant="normal">r</mml:mi></mml:mrow><mml:mrow><mml:mn>3</mml:mn><mml:mo>+</mml:mo></mml:mrow></mml:msup></mml:mrow></mml:math>interactions in single crystals of<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant="normal">Ho</mml:mi></mml:mrow><mml:mrow><mml:mi>x</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant="normal">Y</mml:mi></mml:mrow><mml:mrow><mml:mn>1</mml:mn><mml:mi>−</mml:mi><mml:mi>x</mml:mi></mml:mrow></mml:msub></mml:mrow><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant="normal">VO</mml:mi></mml:mrow><mml:mrow><mml:mn>4</mml:mn></mml:mrow></mml:msub></mml:mrow></mml:math><mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mo>(</mml:mo><mml:mi>x</mml:mi><mml:mo>=</mml:mo><mml:mn>0.02</mml:mn><mml:mn/><mml:mo>–</mml:mo><mml:mn>1</mml:mn><mml:mo>.</mml:mo><mml:mn>0</mml:mn><mml:mn>0</mml:mn><mml:mo>)</mml:mo></mml:math>

2001· article· lv· W2092305791 on OpenAlexafffund
Sushil K. Misra, S. I. Andronenko

Bibliographic record

VenuePhysical review. B, Condensed matter · 2001
Typearticle
Languagelv
FieldChemical Engineering
TopicCatalysis and Oxidation Reactions
Canadian institutionsConcordia University
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsPhysicsElectron paramagnetic resonanceCrystallographyCrystal (programming language)ParamagnetismField (mathematics)Atomic physicsCondensed matter physicsNuclear magnetic resonanceChemistry

Abstract

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Liquid-helium temperature electron paramagnetic resonance (EPR) spectra of the ${\mathrm{Er}}^{3+}$ ion in single crystals of ${\mathrm{Ho}}_{x}{\mathrm{Y}}_{1\ensuremath{-}x}{\mathrm{VO}}_{4}$ $(x=0.02--1.0)$ are exploited to reveal the influence of the crystal-field and ${\mathrm{Er}}^{3+}{\ensuremath{-}\mathrm{H}\mathrm{o}}^{3+}$ interactions. The ${\mathrm{Er}}^{3+}$ g value at 4 K in the lightly doped samples $(x<0.3)$ was here successfully accounted for by the estimated crystal-field parameters ${(\mathrm{c}\mathrm{m}}^{\mathrm{\ensuremath{-}}1}$): ${B}_{2}^{0}=\ensuremath{-}108.0,$ ${B}_{4}^{0}=40.0,$ ${B}_{6}^{0}=\ensuremath{-}40.0,$ ${B}_{4}^{4}=\ensuremath{-}949.0,$ ${B}_{6}^{4}=26.0,$ while that in the concentrated paramagnetic samples $(x=0.9,$ 1.0) by the parameters ${(\mathrm{c}\mathrm{m}}^{\mathrm{\ensuremath{-}}1}$): ${B}_{2}^{0}=\ensuremath{-}114.8,$ ${B}_{4}^{0}=46.9,$ ${B}_{6}^{0}=\ensuremath{-}43.8,$ ${B}_{4}^{4}=\ensuremath{-}971.4,$ ${B}_{6}^{4}=91.9.$ The shift of the ${\mathrm{Er}}^{3+}$ g value in the paramagnetic ${\mathrm{Ho}}_{x}{\mathrm{Y}}_{1\ensuremath{-}x}{\mathrm{VO}}_{4}$ crystals $(x=0.9,$ 1.0) from that in the diamagnetic ${\mathrm{YVO}}_{4}$ crystal has been analyzed to estimate the value of the parameter \ensuremath{\gamma} (=-2.2 ${\mathrm{cm}}^{\mathrm{\ensuremath{-}}1}$) describing the diagonal element of the symmetric tensor representing ${\mathrm{Ho}}^{3+}{\ensuremath{-}\mathrm{E}\mathrm{r}}^{3+}$ interactions. The unresolved EPR linewidth of the ${\mathrm{Er}}^{3+}$ ion is accounted for by the indirect superhyperfine interaction ${(A}_{\ensuremath{\parallel}})$ of the ${\mathrm{Er}}^{3+}$ ion with the surrounding ${}^{165}\mathrm{Ho}$ nuclei, estimating ${A}_{\ensuremath{\parallel}}=0.0026{\mathrm{cm}}^{\mathrm{\ensuremath{-}}1}.$ In addition, the absolute value of the parameter \ensuremath{\varepsilon}, an off-diagonal element of the antisymmetric tensor describing ${\mathrm{Ho}}^{3+}{\ensuremath{-}\mathrm{E}\mathrm{r}}^{3+}$ interactions, has been estimated to be $|\ensuremath{\varepsilon}|=0.029{\mathrm{cm}}^{\mathrm{\ensuremath{-}}1}.$

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.003
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: none
GenreCandidate signal: Empirical · Consensus signal: none
Teacher disagreement score0.316
Threshold uncertainty score0.975

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0010.003
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0010.003
Science and technology studies0.0020.001
Scholarly communication0.0020.003
Open science0.0020.001
Research integrity0.0020.004
Insufficient payload (model declined to judge)0.3160.086

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.018
GPT teacher head0.251
Teacher spread0.233 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations6
Published2001
Admission routes2
Has abstractyes

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