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Record W2093792328 · doi:10.1063/1.1386806

Interaction of short-chain alkane thiols and thiolates with small gold clusters: Adsorption structures and energetics

2001· article· en· W2093792328 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueThe Journal of Chemical Physics · 2001
Typearticle
Languageen
FieldMaterials Science
TopicNanocluster Synthesis and Applications
Canadian institutionsSteacie Institute for Molecular Sciences
FundersBayer
KeywordsChemistryDensity functional theoryDissociation (chemistry)Gold clusterAb initioComputational chemistryBond-dissociation energyAdsorptionCovalent bondIonic bondingEnergeticsChemical physicsCluster (spacecraft)CrystallographyPhysical chemistryIonThermodynamicsOrganic chemistry

Abstract

fetched live from OpenAlex

Gold–sulfur bonding is investigated theoretically using a variety of electronic structure methods, including the Becke–Perdew semilocal density functional, the B3LYP hybrid approach, the Hartree–Fock method, and the post Hartree–Fock approaches MP2 and QCISD(T). Particular emphasis is given to adsorption structure and energetics in the case of weak and strong interactions of this general type, using up to five gold atoms and up to three carbon atoms in the aliphatic chain. It is found that all methods which take into account electron correlation, including the density functional methods, lead to quite similar structures. Concerning the energetics, the Becke–Perdew functional is found to overbind typically by about 5–15%. Quasiglobal structural relaxation based on ab initio simulated annealing clearly shows that the adsorption of thiolates onto gold clusters results in a dramatic distortion of the cluster framework. From a structural point of view the thiolate sulfur–gold bond has a distinctive directional (covalent) character which results in a clear preference for Au–S–C bond angles in the range of 103.5° and 108.7°. In general, dissociation into open-shell species is preferred against the formation of the ionic closed-shell counterparts if the sulfur–gold bond is forced to break. However, neutral closed-shell products can be favored if fragmentation of the gold cluster is allowed for as a dissociation channel. Finally, it is demonstrated that using ethyl or n-propyl chains instead of the methyl group leads to only small changes of the binding energies.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.006
Threshold uncertainty score0.192

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.243
Teacher spread0.223 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it