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Record W2108871623 · doi:10.1002/ejic.200901126

Reactivity Pattern in the Room‐Temperature Activation of NH<sub>3</sub> by the Main‐Group Atomic Ions Ga<sup>+</sup>, Ge<sup>+</sup>, As<sup>+</sup> and Se<sup>+</sup>

2010· article· en· W2108871623 on OpenAlexaff
Gregory K. Koyanagi, Vitaliy Kapishon, Diethard K. Böhme, Xinhao Zhang, Helmut Schwarz

Bibliographic record

VenueEuropean Journal of Inorganic Chemistry · 2010
Typearticle
Languageen
FieldChemical Engineering
TopicAmmonia Synthesis and Nitrogen Reduction
Canadian institutionsYork University
Fundersnot available
KeywordsChemistryReactivity (psychology)IonAmmoniaKinetic energyProtonActivation energyHydrogenChemical kineticsKineticsHydrogen atomYield (engineering)Physical chemistryInorganic chemistryAnalytical Chemistry (journal)Group (periodic table)Organic chemistry

Abstract

fetched live from OpenAlex

Abstract The activation of ammonia by the main‐group cations Ga + , Ge + , As + and Se + has been explored both experimentally and theoretically. ICP/SIFT tandem mass spectrometer measurements of room‐temperature kinetics have revealed a substantial variation in rates and product distributions across the Periodic Table of Elements. The main features of the observed primary chemistry include H‐atom elimination, ammonia addition and a cation‐assisted proton transfer to yield NH 4 + that is second order in ammonia. These observations are shown to be completely consistent with computed potential energy surfaces for the reactions of each of the four atomic cations. Dehydrogenation by the elimination of molecular hydrogen, not observed experimentally, is shown by the calculations to be inhibited by the presence of a kinetic barrier.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.003
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow), Research integrity
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.011
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0030.001
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.001
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0010.004
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.191
Teacher spread0.186 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations18
Published2010
Admission routes1
Has abstractyes

Explore more

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