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Record W2130532675 · doi:10.1002/cphc.200900024

Guest–Host Hydrogen Bonding in Structure H Clathrate Hydrates

2009· article· en· W2130532675 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueChemPhysChem · 2009
Typearticle
Languageen
FieldEnvironmental Science
TopicMethane Hydrates and Related Phenomena
Canadian institutionsUniversity of British ColumbiaSteacie Institute for Molecular Sciences
Fundersnot available
KeywordsClathrate hydrateChemistryHydrogen bondMoleculeCrystallographyHydrogenRelaxation (psychology)CageEtherMolecular dynamicsDiphenyl etherComputational chemistryHydrateOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Molecular dynamics simulations of the structure H (sH) clathrate of tert ‐butylmethylether show the prevalence of ether–water hydrogen bonding (see picture), absent in the neo‐hexane sH clathrate. This affects guest–cage dynamics and host–water dielectric relaxation dynamics. The 13 C and 1 H NMR relaxation times for both guests are measured, and the differences are explained in terms of guest–host interactions in the two clathrates. magnified image The formation of guest–host hydrogen bonds in structure H (sH) clathrate hydrates is studied herein. We contrast the structure and guest dynamics of the tert‐ butylmethylether (TBME) and neohexane (NH) sH clathrates by performing molecular dynamics simulations on these two clathrates and measuring 1 H and 13 C NMR relaxation times of the guests. These two guests are isoelectronic and differ with respect to the presence of the ether oxygen atom in TBME and a CH 2 group in NH. The TBME guest forms long‐lived hydrogen bonds with water molecules in the equatorial region of the large sH clathrate cage. These hydrogen bonds effectively tether the TBME guest to the side of the cage and restrict its rattling and rotational motions in the cage compared to NH, which does not become hydrogen bonded to the cage’s water molecules.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.030
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.220
Teacher spread0.212 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it