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Record W2131770563 · doi:10.1002/chem.200390240

Cover Picture: Coordination Algorithms Control Molecular Architecture: [Cu<sup>I</sup><sub>4</sub>(L2)<sub>4</sub>]<sup>4+</sup> Grid Complex Versus [M<sup>II</sup><sub>2</sub>(L2)<sub>2</sub>X<sub>4</sub>]<sup>y+</sup> Side‐By‐Side Complexes (M=Mn, Co, Ni, Zn; X=Solvent or Anion) and [Fe<sup>II</sup>(L2)<sub>3</sub>][Cl<sub>3</sub>Fe<sup>III</sup>OFe<sup>III</sup>Cl<sub>3</sub>] (Chem. Eur. J. 16/2003)

2003· paratext· en· W2131770563 on OpenAlexaff
Yanhua Lan, Dietmar Kennepohl, Boujemaa Moubaraki, Keith S. Murray, J.D. Cashion, Geoffrey B. Jameson, Sally Brooker

Bibliographic record

VenueChemistry - A European Journal · 2003
Typeparatext
Languageen
FieldMedicine
TopicMetal complexes synthesis and properties
Canadian institutionsAthabasca University
Fundersnot available
KeywordsOctahedronCrystallographyChemistryCopperLigand (biochemistry)IonTetrahedronCobaltCover (algebra)Metal ions in aqueous solutionPyridazineMetalStereochemistryCrystal structureInorganic chemistry

Abstract

fetched live from OpenAlex

Abstract The cover picture shows how differing coordination algorithms control the molecular architecture of complexes of the pyridazine‐containing, two‐armed, acyclic Schiff base ligand L2 (left, prepared from one equivalent of 3,6‐diformylpyridazine and two equivalents of d‐anisidine). Two very different complexes of L2 self‐assemble from tetrahedral copper(I) versus octahedral zinc(II), nickel(II), and cobalt(II) controlled 1 : 1 reactions with L2. In both cases the metal ions are bridged by the pyridazine moieties in L2, but in the case of the tetrahedral copper(II) the result is a tetrametallic [2×2] grid complex ([CuI4(L2)4]4+: top right), whilst in the case of the octahedral metal(II) ions dimetallic side‐by‐side complexes, [MII2(L2)2(X)4]y+ (M = Mn, Co, Ni, Zn; X = solvent or anion), are formed (bottom right). The cover image was kindly generated by M. Crawford (University of Otago) with Strata Studio Pro (Strata). More details are given by S. Brooker and co‐workers on p. 3772 ff.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Not applicable · Consensus signal: none
GenreCandidate signal: Other · Consensus signal: none
Teacher disagreement score0.050
Threshold uncertainty score0.166

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.001
Open science0.0010.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0500.004

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.241
Teacher spread0.219 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designNot applicable
Domainnot available
GenreOther

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2003
Admission routes1
Has abstractyes

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Same venueChemistry - A European JournalSame topicMetal complexes synthesis and propertiesFrench-language works237,207