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Record W2135163361 · doi:10.1002/cjce.22320

Fabrication and evaluation of acrylated epoxidized castor oil‐toughened diglycidyl ether of bisphenol A nanocomposites

2015· article· en· W2135163361 on OpenAlexvenueno aff
Nagarjuna Reddy Paluvai, Smita Mohanty, Sanjay K. Nayak

Bibliographic record

VenueThe Canadian Journal of Chemical Engineering · 2015
Typearticle
Languageen
FieldMaterials Science
TopicPolymer composites and self-healing
Canadian institutionsnot available
FundersDepartment of Chemicals and Petrochemicals, Ministry of Chemicals and Fertilizers, India
KeywordsDiglycidyl etherEpoxyCastor oilThermogravimetric analysisMaterials scienceDynamic mechanical analysisFlexural strengthGlass transitionDifferential scanning calorimetryFlexural modulusComposite materialNanocompositeUltimate tensile strengthEpoxidized soybean oilBisphenol APolymerChemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract Castor oil‐based epoxy monomer was prepared using a two‐step approach: epoxidation of castor oil, followed by acrylation of epoxidized castor oil. A bio‐based diglycidyl ether of bisphenol A (DGEBA) epoxy nanocomposites was prepared by the incorporation of organo‐modified montmorillonite (OMMT) clay to the DGEBA/AECO system. The cured bio‐based DGEBA epoxy nanocomposites at 0.80:0.2:0.001 g/g exhibited higher tensile strength (56 MPa), tensile modulus (1933 MPa), flexural strength (132 MPa), flexural modulus (2518 MPa), elongation (23.1 %), and impact strength (34 kJ/m 2 ). The nanocomposites at 0.6:0.4:0.001 g/g can easily bend up to 360° without any damage; similarly, the 0.8:0.2:0.001 g/g system can bend up to 180°. Thermal behaviour of the bio‐based epoxy systems was characterized by differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), and dynamic mechanical analysis (DMA). The obtained nanocomposites displayed a higher char yield (8.9 %) at 700 °C and glass transition temperature (108 °C) than the DGEBA/AECO systems. Further SEM analysis was used to study the morphological changes in the fractured surfaces of bio‐based epoxy systems, which reveals that crack propagation decreases with addition of AECO to the DGEBA epoxy system.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.024
Threshold uncertainty score0.292

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.025
GPT teacher head0.238
Teacher spread0.213 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations29
Published2015
Admission routes1
Has abstractyes

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