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Record W2148976803 · doi:10.1021/jp011627m

Oxidation Reactions of Lanthanide Cations with N<sub>2</sub>O and O<sub>2</sub>:  Periodicities in Reactivity

2001· article· en· W2148976803 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueThe Journal of Physical Chemistry A · 2001
Typearticle
Languageen
FieldMaterials Science
TopicCatalytic Processes in Materials Science
Canadian institutionsYork University
Fundersnot available
KeywordsLanthanideChemistryArrhenius equationReactivity (psychology)IonAnalytical Chemistry (journal)Inductively coupled plasmaPhysical chemistryActivation energyInorganic chemistryPlasma

Abstract

fetched live from OpenAlex

The oxidation reactions of all of the lanthanide cations (except Pm + ) with N 2 O and O 2 have been investigated using the inductively coupled plasma selected-ion flow tube (ICP/SIFT) technique. Lanthanide cations were generated in an inductively coupled plasma (ICP) ion source. Observations are reported for the reactions of La +, Ce +, Pr +, Nd +, Sm +, Eu +, Gd +, Tb +, Dy +, Ho +, Er +, Tm +, Yb +, and Lu + with N 2 O and O 2 at room temperature (295 ± 2 K) in helium at a total pressure of 0.35 ± 0.02 Torr. Measured reaction rates varied from close to the predicted ion−molecule collision rate down to less than 0.1% efficiency. Observations are rationalized in terms of reaction thermodynamics and electronic structure effects. The efficiency for the reactions with N 2 O was found to decrease as the energy required to promote the metal-ion electron from the 4f n 5d 0 6s 1 to the 4f n -1 5d 1 6s 1 configuration increases. Remarkable and different Arrhenius-like correlations are found in the N 2 O reactivity of the early and late lanthanide cations with this electron promotion energy.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.347

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.234
Teacher spread0.224 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it