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Record W2149216087 · doi:10.1002/polb.21893

<i>PVT</i> properties of linear and dendritic polymers

2009· article· en· W2149216087 on OpenAlexaffabout
Robert Simha, Leszek A. Utracki

Bibliographic record

VenueJournal of Polymer Science Part B Polymer Physics · 2009
Typearticle
Languageen
FieldMaterials Science
TopicDendrimers and Hyperbranched Polymers
Canadian institutionsNational Research Council Canada
Fundersnot available
KeywordsDendrimerThermodynamicsCompressibilityPolystyreneThermal expansionChemistryPolymerEtherPolymer chemistryExcluded volumeVolume (thermodynamics)Equation of stateLinear polymerMaterials sciencePhysical chemistryPhysicsOrganic chemistry

Abstract

fetched live from OpenAlex

Abstract The aim of this article is to examine the limits of applicability of the Simha‐Somcynsky (S‐S) equation of state (EOS) by comparing the pressure‐volume‐temperature ( PVT ) data and the derivatives (compressibility, κ, and thermal expansion coefficient, α) of anionic linear polystyrene (PS) with poly(benzyl ether) dendrimers (PBED). Fitting the PVT of PBED data to the S‐S EOS was similarly satisfactory as that of PS and the computed Lennard‐Jones (L‐J) interaction parameters showed similar errors of ca. 1%. Next, the experimental derivatives, α and κ of PS and PBED were compared with these functions computed from the S‐S EOS—good agreement was obtained for α at ambient pressure, P , indicating validity of the S‐S theory at least up to the first derivative. While the predicted κ = κ( P ) dependence for PS and a linear PBED homologue was correct, for dendrimers the compressibility was higher at low pressure and it was lower at high P than theory predicts. Also the extracted values of the L‐J repulsion volume, v *, between a segment pair was smaller than expected. The specific architecture of dendrimer molecules is responsible for this behavior, since their 3D configuration is significantly different from the S‐S model with uniform segmental density and oxygen bonds in the main and side chains add flexibility. © 2009 NRC Canada. J Polym Sci Part B: Polym Phys 48: 322–332, 2010

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.039
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.002
Scholarly communication0.0000.002
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.249
Teacher spread0.229 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations6
Published2009
Admission routes2
Has abstractyes

Explore more

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