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Record W2160438242 · doi:10.1002/jsfa.2339

A new technology for extraction and purification of proanthocyanidins derived from sea buckthorn bark

2005· article· en· W2160438242 on OpenAlex
Bijun Xie, Siyi Pan, Yang Er-ning, Kexin Wang, Stefan Cenkowski, Arnie W Hydamake, S. Ananda Rao

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueJournal of the Science of Food and Agriculture · 2005
Typearticle
Languageen
FieldMedicine
TopicPhytochemical and Pharmacological Studies
Canadian institutionsUniversity of Manitoba
Fundersnot available
KeywordsProanthocyanidinChemistryExtraction (chemistry)ChromatographyBark (sound)DesorptionAdsorptionHigh-performance liquid chromatographyEthanolYield (engineering)Central composite designPolyphenolResponse surface methodologyOrganic chemistryMaterials scienceAntioxidant

Abstract

fetched live from OpenAlex

Abstract A new technology involving resin purification of proanthocyanidins extracted from sea buckthorn bark has been studied. By investigating single‐factor effects, the main factors affecting proanthocyanidin extraction were identified as extraction temperature, pH and ethanol concentration. A central composite design and response surface analysis were used to determine the optimal parameters of the extraction process (temperature 21 °C, pH 5.13, ethanol concentration 65%). The optimal resin for purification, D3520, was selected from 16 different resins by means of static adsorption and dynamic adsorption/desorption tests. After using this resin to purify the crude extract, a proanthocyanidin extract was obtained whose yield and purity were above 80% and greater than 95% respectively. Procyanidin dimers and trimers predominated among oligomer procyanidins of the proanthocyanidin extract according to analyses by high‐performance liquid chromatography (HPLC) and HPLC/mass spectrometry. Copyright © 2005 Society of Chemical Industry

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.036
Threshold uncertainty score0.075

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.020
GPT teacher head0.283
Teacher spread0.263 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it