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Record W2162163218 · doi:10.1002/ejic.200800880

The Variable Strength of the Sulfur–Sulfur Bond: 78 to 41 kcal – G3, CBS‐Q, and DFT Bond Energies of Sulfur (S<sub>8</sub>) and Disulfanes XSSX (X = H, F, Cl, CH<sub>3</sub>, CN, NH<sub>2</sub>, OH, SH)

2009· article· en· W2162163218 on OpenAlexaff
Michael Denk

Bibliographic record

VenueEuropean Journal of Inorganic Chemistry · 2009
Typearticle
Languageen
FieldChemistry
TopicFree Radicals and Antioxidants
Canadian institutionsUniversity of Guelph
Fundersnot available
KeywordsSulfurChemistryBond energyBond strengthBond orderBond lengthSingle bondThree-center two-electron bondComputational chemistryMoleculeSextuple bondDelocalized electronElectron delocalizationRange (aeronautics)Organic chemistryMaterials scienceGroup (periodic table)

Abstract

fetched live from OpenAlex

Abstract Experimental values for the strength of the sulfur–sulfur bond scatter over a wide range and are frequently in disagreement with each other. For S 8 , reliable experimental data seem to lack entirely. To check experimental data and establish the strength of the sulfur–sulfur bond in S 8 , high‐precision thermochemical calculations (G3, CBS‐Q) and DFT methods were employed. The calculations confirm a stunning range for the strength of the sulfur–sulfur bond with energies between 77.7 kcal for FSSF and only 41.8 kcal for tetrasulfane, HSS–SSH. For the pivotal bond energy of elemental sulfur, S 8 , the bond energy is 40.5 kcal but can be narrowed to 38.0–39.2 kcal mol –1 by including CBS‐QB3 data. While older DFT methods are not well suited to accurately reproduce the S–S bond energies, excellent data can be obtained with the recently introduced Boese–Martin (BMK) hybrid DFT method. Atoms in molecules (AIM) calculations reveal significant multiple bonding and spin delocalization in the sulfur radicals XS · . (© Wiley‐VCH Verlag GmbH &amp; Co. KGaA, 69451 Weinheim, Germany, 2009)

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.007
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.001
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.001
Scholarly communication0.0000.000
Open science0.0010.001
Research integrity0.0000.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.005
GPT teacher head0.188
Teacher spread0.182 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations38
Published2009
Admission routes1
Has abstractyes

Explore more

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