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Record W2311212307 · doi:10.1021/acs.iecr.5b00806

Role of Liquid Concentration in Coke Yield from Model Vacuum Residue–Coke Agglomerates

2015· article· en· W2311212307 on OpenAlexafffund
Deepesh Kumar, Christa E. Müller, Peter Pfeifer, Jason Wiens, Jennifer McMillan, Michael Wormsbecker, Craig A. McKnight, Murray R. Gray

Bibliographic record

VenueIndustrial & Engineering Chemistry Research · 2015
Typearticle
Languageen
FieldChemistry
TopicPetroleum Processing and Analysis
Canadian institutionsSyncrude (Canada)University of Alberta
FundersNatural Sciences and Engineering Research Council of CanadaSyncrude
KeywordsCokeAgglomerateYield (engineering)Fraction (chemistry)ChemistryMaterials scienceResidue (chemistry)MetallurgyChromatographyComposite materialOrganic chemistry

Abstract

fetched live from OpenAlex

The fluid coking process is an example of an upgrading process that uses hot solids to heat and crack bitumen into more valuable products. When feed liquid is sprayed into a fluid bed of hot solids, the solids tend to agglomerate, giving simultaneous heating, reaction, and disintegration processes. The reaction of mixtures of three Athabasca vacuum residues and fluid coke particles was investigated by heating them in Curie point reactors in an induction furnace up to 530 °C. Small scale reactors with machined wells were fabricated from Curie point alloy. The yield of coke was measured as a function of the ratio of liquid to solid, heating rate, and feed type. Coke yields were insensitive to heating rates from 5 to 120 °C/s, at a constant final temperature. Bubbling was observed as the ratio of liquid feed in the mixture was raised above a threshold, depending on the reactivity of the feed used. Bubbling was observed to increase with greater heating rates, but it had little effect on ultimate coke yield. Coke yield increased with the fraction of bitumen on particles for all feed types tested. When the coke yields were normalized using the microcarbon residue content of the feeds, the results did not give a single trend when plotted with fraction of feed present in the mixtures.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0010.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.102
GPT teacher head0.317
Teacher spread0.216 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations7
Published2015
Admission routes2
Has abstractyes

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