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Record W2314242529 · doi:10.1021/jp507142v

Dispersion Stability, Ligand Structure and Conformation, and SERS Activities of 1-Alkanethiol Functionalized Gold and Silver Nanoparticles

2014· article· en· W2314242529 on OpenAlexaff
Siyam M. Ansar, Manuel Gadogbe, Kumudu Siriwardana, Jane Y. Howe, Stas Dogel, Hooman Hosseinkhannazer, Willard E. Collier, J.M. Doña-Rodrı́guez, Shengli Zou, Dongmao Zhang

Bibliographic record

VenueThe Journal of Physical Chemistry C · 2014
Typearticle
Languageen
FieldMaterials Science
TopicGold and Silver Nanoparticles Synthesis and Applications
Canadian institutionsNorcada (Canada)Hitachi (Canada)
FundersOffice of Experimental Program to Stimulate Competitive ResearchDivision of ChemistryOffice of Naval ResearchNational Science Foundation
KeywordsColloidal goldDispersion stabilityDispersion (optics)Ligand (biochemistry)ChemistryCarbon fibersNanoparticleSilver nanoparticleCarbon chainNanotechnologyCrystallographyMaterials scienceOrganic chemistryComposite materialPhysics

Abstract

fetched live from OpenAlex

Dispersion stability, ligand structure and conformation, and SERS activities of 1-alkanethiol (C n H 2 n +1 SH, n = 2–14) functionalized gold and silver nanoparticles (AuNPs and AgNPs) were studied as a function of alkanethiol carbon chain length and nanoparticle (NP) type and size. The dispersion stability of alkanethiol functionalized NPs in water increases with increasing alkanethiol chain length and NP size, and the stabilities of the alkanethiol-containing AuNPs are higher than their AgNP counterparts. C 3 H 7 SH and longer alkanethiols are highly ordered on AgNPs but disordered on AuNPs. The SERS intensity of the C–S stretch band for the model alkanethiols on AgNPs and AuNPs decays exponentially ( I = I 0 exp(− N c / N 0 )) with increasing number of carbon atoms ( N c ). The empirical decay length N 0, in terms of the number of the carbon atoms, is 1.29, 0.53, and 0.10 for AgNPs with diameters of 50, 30, and 10 nm, respectively. This decay length is less than 1 for AuNPs of difference sizes. These results show that changing the NP gap size by a distance equivalent to a single chemical bond can have a significant impact on the NP integrated SERS activities.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.003
Threshold uncertainty score0.155

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.212
Teacher spread0.204 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations27
Published2014
Admission routes1
Has abstractyes

Explore more

Same venueThe Journal of Physical Chemistry CSame topicGold and Silver Nanoparticles Synthesis and ApplicationsFrench-language works237,207