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Record W2315577556 · doi:10.1021/jf304439s

Characterization of Trilayer Antimicrobial Diffusion Films (ADFs) Based on Methylcellulose–Polycaprolactone Composites

2013· article· en· W2315577556 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueJournal of Agricultural and Food Chemistry · 2013
Typearticle
Languageen
FieldChemistry
TopicAntimicrobial agents and applications
Canadian institutionsFPInnovationsInstitut National de la Recherche Scientifique
Fundersnot available
KeywordsPolycaprolactoneAntimicrobialFourier transform infrared spectroscopyMaterials scienceUltimate tensile strengthDiffusionCelluloseComposite materialChemical engineeringAgar diffusion testChemistryPolymerOrganic chemistryBiochemistry

Abstract

fetched live from OpenAlex

Novel trilayer antimicrobial diffusion films (ADFs) were developed for food applications. ADFs were composed of two external layers of polycaprolactone and one internal layer of nanocrystalline cellulose (NCC)-reinforced methylcellulose (MC) matrix. Two antimicrobial mixtures (formulations A and B) were incorporated in the MC layer and compared via the evaluation of film properties. Resulting ADFs were inserted as diffusion devices into vegetable packages, and samples were stored at 4 °C for 14 days. Microbiological diffusion assays in the presence of ADFs were performed on pathogenic bacteria. From this, the study focused on characterizing the structural, physicochemical properties and total phenols (TP) release from ADFs. This TP release was determined by Folin-Ciocalteu's method and by FTIR analysis. Results indicated a controlled release of antimicrobials into the headspace (16.5% for formulation A and 13.4% for formulation B). Good correlations (≥90%) between both methods allowed validating an innovative, accurate, rapid FTIR procedure to quantify the diffusion of TP. SEM micrographs showed fibrillar structure due to NCC and a more compact network due to antimicrobials. Encapsulated antimicrobial formulations induced color changes without affecting visual attributes of films. ADFs containing formulation B exhibited the highest tensile strength (17.3 MPa) over storage.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.011
Threshold uncertainty score0.744

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.186
Teacher spread0.179 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it