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Record W2315858771 · doi:10.1139/v2012-068

Formal transfer potentials of strontium and uranyl ions at water|1,2-dichloroethane interfaces

2012· article· en· W2315858771 on OpenAlexaffvenue
Anne-Marie Montgomery, Zhifeng Ding

Bibliographic record

VenueCanadian Journal of Chemistry · 2012
Typearticle
Languageen
FieldChemistry
TopicElectrochemical Analysis and Applications
Canadian institutionsWestern University
FundersSchweizerischer Nationalfonds zur Förderung der Wissenschaftlichen Forschung
KeywordsChemistryUranylStrontiumAqueous solutionPolarographyIonElectrochemistryLigand (biochemistry)Mass transferITIESExtraction (chemistry)Metal ions in aqueous solutionAnalytical Chemistry (journal)Inorganic chemistryPhysical chemistryCyclic voltammetryOrganic chemistryChromatography

Abstract

fetched live from OpenAlex

The extraction of dioxouranium (UO 2 2+ ), or uranyl, and strontium (Sr 2+ ) ions from spent nuclear fuel (SNF), often through a biphasic (aqueous / organic solvent) ligand assisted process, is critical for the implementation of a closed-loop nuclear fuel cycle whereby SNF is diverted from permanent geological disposal and the life of the nuclear industry is extended. Deeper understanding of the biphasic extraction process can be achieved through facile electrochemical experiments at a liquid|liquid interface. Of primary importance to developing a quantitative analysis of the ligand assisted or facilitated ion transfer (FIT) (i.e., transfer through interfacial complexation) case is to first quantify the free or simple metal IT; that is the amount of applied potential required to “push” ions across the water|organic interface. This value is, in fact, a constant referred to as the formal transfer potential ([Formula: see text]), which is unique to each metal ion in the biphasic system. Because of their hydrophilicity they often limit the polarizable potential window. Values for [Formula: see text], for the most part, have only been estimated. With a microinterface housed at the tip of a 25 µm capillary it is possible to reduce the Faradaic current to observe their transfer. Herein is described the quantification of [Formula: see text] and [Formula: see text] or the formal transfer potentials for dioxouranium and strontium ions, respectively.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesInsufficient payload (model declined to judge)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.004
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.007
GPT teacher head0.195
Teacher spread0.188 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations11
Published2012
Admission routes2
Has abstractyes

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