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Record W2316632302 · doi:10.1107/s0108767310098090

Temperature-dependent structural changes and hydration of CsLiB<sub>6</sub>O<sub>10</sub>

2010· article· en· W2316632302 on OpenAlexaff
Natalia Sennova, Р. С. Бубнова, G. CORDIER, Barbara Albert, С. К. Филатов, L. I. Isaenko, L. Gubenko

Bibliographic record

VenueActa Crystallographica Section A Foundations of Crystallography · 2010
Typearticle
Languageen
FieldMaterials Science
TopicCrystal Structures and Properties
Canadian institutionsUniversity of New Brunswick
Fundersnot available
KeywordsCrystallographyMaterials scienceThermodynamicsChemistryPhysics

Abstract

fetched live from OpenAlex

This presentation features a combined photo-crystallography and Density Functional Theory study on two Ru-based complexes that have potential application in optical data storage [1]. Solid-state linkage photo-isomerism is the transformative process, that yields a binary structural signature from 0 (ground-state) to 1 (the photo-isomer) [2]. The compounds are based on the general series of materials, [Ru(SO 2 )(NH 3 ) 4 X]Y, where X is trans to the SO 2 ligand. In this particular study, X = isonicotinamide, Y = tosylate 2 ; X = H 2 O and Y = camphorsulfonate. The SO 2 is the photoactive ligand, converting from S-end bound ( 1 ) to side-bound ( 2 ) coordination with the Ru metal centre [3]. Photo-crystallography experiments reveal the 3-D geometry of these light-activated molecular species [4], with up to 27% photoconversion efficiency. Complementary DFT calculations quantify a relationship between the photoconversion fraction and the size of the reaction cavity, i.e. the void surrounding the SO 2 ligand within the crystal lattice. The associated energetics of the ligand photoisomerism are presented in tandem with these findings. The relevance of these findings to the optical data storage industry are discussed; in particular, their role in helping to solve the current challenges in securing suitable materials for industrial application. This leads to the ultimate goal of being able to tailor an optoelectronic material for a given device application.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.001
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.041
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0010.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0010.001
Science and technology studies0.0010.001
Scholarly communication0.0000.001
Open science0.0000.000
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.008
GPT teacher head0.220
Teacher spread0.212 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations0
Published2010
Admission routes1
Has abstractyes

Explore more

Same venueActa Crystallographica Section A Foundations of CrystallographySame topicCrystal Structures and PropertiesFrench-language works237,207