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Record W2318005902 · doi:10.1002/poc.3320

Conformation/Tautomerization effect on the pK<sub>a</sub> values of lumazine and 6‐thienyllumazine

2014· article· en· W2318005902 on OpenAlexafffund
Akef T. Afaneh, Georg Schreckenbach

Bibliographic record

VenueJournal of Physical Organic Chemistry · 2014
Typearticle
Languageen
FieldChemistry
TopicFree Radicals and Antioxidants
Canadian institutionsUniversity of Manitoba
FundersNatural Sciences and Engineering Research Council of Canada
KeywordsTautomerChemistryConformational isomerismDeprotonationComputational chemistryDensity functional theoryAqueous solutionSolvationTriazineStereochemistryCrystallographyIonPhysical chemistryMoleculeOrganic chemistry

Abstract

fetched live from OpenAlex

Density functional theory [B3LYP/6‐311+G(d,p)] was used in combination with the conductor‐like polarizable continuum model (CPCM) solvation model to investigate the relative stability and site‐specific values of neutral and ionized tautomers of lumazine (LM) and 6‐thienylLM (TLM). Two types of populations should be taken into consideration when calculating the , tautomers, and conformers. The major tautomer of neutral LM in aqueous solution is 13‐LM (the 13 notation refers to the acidic protons being in positions 1 and 3 of LM) TLM has decreased acidity at N 8 relative to LM. Further, the trans conformer of TLM is more acidic than cis . Similar to the case of LM, for TLM, N 1 is more acidic than N 3 in the uracil part. However, N 8 is predicted to be a stronger acid than N 1 for TLM. This acidity enhancement is essentially because of a specific stabilization of the anion when the thienyl group replaces H. Two factors are responsible for the acidity strength of N 8 : The thienyl ring upon deprotonation acts inductively as an electron‐withdrawing group, and the excess electron density is dispersed better when the system is trans and contains second‐row atoms. Accurate pK a calculation requires that all conformers/tautomers be included into the calculation. Copyright © 2014 John Wiley &amp; Sons, Ltd.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.005
Threshold uncertainty score0.444

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.003
GPT teacher head0.196
Teacher spread0.193 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations3
Published2014
Admission routes2
Has abstractyes

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