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Record W2321121031 · doi:10.1021/la4018932

Controlled 2D Organization of Gold Nanoparticles in Block Copolymer Monolayers

2013· article· en· W2321121031 on OpenAlex
Samuel Lamarre, Cynthia Lemay, Charles Labrecque, Anna M. Ritcey

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueLangmuir · 2013
Typearticle
Languageen
FieldMaterials Science
TopicBlock Copolymer Self-Assembly
Canadian institutionsUniversité Laval
Fundersnot available
KeywordsCopolymerNanoparticleRadius of gyrationPolymerMonolayerMaterials scienceMicelleMorphology (biology)Chemical engineeringNanotechnologyColloidal goldChemical physicsRADIUSSPHERESPolymer chemistryChemistryComposite materialAqueous solutionOrganic chemistry

Abstract

fetched live from OpenAlex

The organization of organic-capped gold nanoparticles in PS-b-PMMA monolayers is investigated. The preferred location of the particles within the block copolymer template is found to depend on both nanoparticle size and the length of the aliphatic capping agent. In the case of relatively short ligands, the particles behave as hard spheres and their incorporation in the polymer matrix can be qualitatively rationalized by entropic considerations. Three distinct arrangements are observed. Particles that are small, relative to the radius of gyration of the host polymer, evenly disperse within the PS domains, whereas the largest particles are considered form ordered, island-like aggregates. Particles of intermediate size exhibit the most striking arrangement, being relegated to the PS-PMMA interface to form organized ring structures. The tendency of these particles to assemble at the interface is sufficiently strong to force a modification of the polymer morphology to accommodate the particles at higher loadings. As the number of particles is increased, the circular PS-b-PMMA surface micelles elongate to form nanostrands.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score0.856

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.001

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.006
GPT teacher head0.207
Teacher spread0.201 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it