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Record W2322247145 · doi:10.1021/cg400552a

Tailoring of Single-Crystalline Complex Ta<sub>5</sub>Si<sub>3</sub> Nanostructures: From Networked Nanowires to Nanosheets

2013· article· en· W2322247145 on OpenAlex
Mohammad Norouzi Banis, Yong Zhang, Qiangfeng Xiao, Mei Cai, Ruying Li, Xueliang Sun

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.

Bibliographic record

VenueCrystal Growth & Design · 2013
Typearticle
Languageen
FieldPhysics and Astronomy
TopicSemiconductor materials and interfaces
Canadian institutionsWestern University
Fundersnot available
KeywordsNanowireNanostructureMaterials scienceChemical vapor depositionNanotechnologyTransmission electron microscopyScanning electron microscopeHigh-resolution transmission electron microscopyChemical engineeringComposite material

Abstract

fetched live from OpenAlex

Single-crystalline Ta 5 Si 3 nanostructures with a complex morphology were synthesized through a catalyst-free, chemical vapor deposition method under low pressures. The morphology, structure, and composition of deposited nanostructures were studied by scanning electron microscopy, X-ray diffraction, and high-resolution transmission electron microscopy. These nanostructures have lengths of up to several tens of micrometers and an average thickness of 13 nm. It was found that the formation of networked Ta 5 Si 3 nanostructures is highly sensitive to the vapor pressure of tantalum chloride and silica and is based on a vapor–solid mechanism. Results indicate that, with the decrease of silica vapor pressure, the Ta 5 Si 3 networked nanowires evolve into networked nanoribbons and nanosheets via two-dimensional growth. Cyclic voltammetry measurements of the Ta 5 Si 3 nanostructures show superior electrochemical capacitance properties of nanosheets compared to nanowires. It is expected that these nanostructures have great potential applications for nanodevices in electronic and energy related applications.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.010
Threshold uncertainty score1.000

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.028
GPT teacher head0.217
Teacher spread0.190 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it