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Record W2323389167 · doi:10.1021/la200153n

Discovery of the Potential of Minimum Mass for Platinum Electrodes

2011· article· en· W2323389167 on OpenAlexaff
Gregory Jerkiewicz, Gholamreza Vatankhah, Shin‐ichi Tanaka, Jean Lessard

Bibliographic record

VenueLangmuir · 2011
Typearticle
Languageen
FieldChemistry
TopicElectrochemical Analysis and Applications
Canadian institutionsUniversité de SherbrookeQueen's University
Fundersnot available
KeywordsPlatinumChemistryElectrochemistryElectrolyteAqueous solutionQuartz crystal microbalanceAnalytical Chemistry (journal)MonolayerElectrodeInorganic chemistryAdsorptionElectrode potentialPhysical chemistryCatalysisOrganic chemistry

Abstract

fetched live from OpenAlex

Electrochemical quartz-crystal nanobalance (EQCN) analysis of the behavior of Pt in aqueous H(2)SO(4) reveals that the interfacial mass reaches a minimum, the potential of minimum mass (E(pmm)), at 0.045 V. A similar behavior is observed for Pt in aqueous HClO(4) and NaOH. E(pmm) is a new parameter describing the electrochemical interface. The value of E(pmm) coincides with the completion of the saturation layer of electroadsorbed H (H(UPD)) and the commencement of H(2)(g) generation or H(2)(g) electro-oxidation. The value of E(pmm) and the structure of the Pt/electrolyte interface are discussed in terms of the interactions of the anions H(3)O(+), H(UPD), H(OPD), and H(2)O with Pt. The layer of H(UPD) embedded in the Pt surface lattice minimizes the surface dipole-water dipole and surface charge-water dipole interactions, thus reduces the wetting ability of Pt. Consequently, the discharge of H(3)O(+) in the electrolytic formation of H(2)(g) or the dissociative adsorption of H(2)(g) that precedes its electro-oxidation to H(3)O(+) proceed easily on Pt, because the species do not have to displace H(2)O molecules. Effective and inexpensive non-platinum electrocatalysts for the electrolytic H(2)(g) generation in water electrolyzers or H(2)(g) electro-oxidation in polymer electrolyte membrane fuel cells should mimic the interfacial behavior of Pt by minimizing the interaction of H(2)O molecules with the electrode.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.002
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.002
Threshold uncertainty score0.006

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.002
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0010.000
Science and technology studies0.0000.001
Scholarly communication0.0010.001
Open science0.0010.001
Research integrity0.0010.001
Insufficient payload (model declined to judge)0.0020.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.010
GPT teacher head0.212
Teacher spread0.202 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations37
Published2011
Admission routes1
Has abstractyes

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