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Record W2326730900 · doi:10.1021/ef101230g

Metal Oxide Nanoparticles for Asphaltene Adsorption and Oxidation

2011· article· en· W2326730900 on OpenAlexaff
Nashaat N. Nassar, Azfar Hassan, Pedro Pereira‐Almao

Bibliographic record

VenueEnergy & Fuels · 2011
Typearticle
Languageen
FieldChemistry
TopicPetroleum Processing and Analysis
Canadian institutionsUniversity of Calgary
Fundersnot available
KeywordsAsphalteneAdsorptionThermogravimetric analysisNanoparticleOxideCatalysisLangmuir adsorption modelInorganic chemistryMetalChemistryChemical engineeringNon-blocking I/OMaterials scienceOrganic chemistry

Abstract

fetched live from OpenAlex

This study investigates the adsorption and oxidation of asphaltenes onto nanoparticles. Six different metal oxide nanoparticles were employed, namely, Fe 3 O 4, Co 3 O 4, TiO 2, MgO, CaO, and NiO. Batch adsorption experiments were carried out at different initial asphaltene concentrations. Asphaltene adsorption was evaluated by measuring the asphaltene concentration using thermogravimetric analysis, and adsorption kinetics and isotherms were obtained. For all the six nanoparticles, the isotherm data fitted well to the Langmuir model. Results showed that asphaltene adsorption is metal-oxide-specific and the adsorption capacities of asphaltenes onto the oxides followed the order CaO > Co 3 O 4 > Fe 3 O 4 > MgO > NiO > TiO 2 . Furthermore, oxidation of asphaltene was investigated after adsorption onto NiO nanoparticles. The oxidation temperature of asphaltene decreased by ∼140 °C in the presence of nanoparticles, showing their catalytic effect. The activation energies calculated by the Coats−Redfern method for asphaltene oxidation processes in the absence and presence of NiO nanoparticles were found to be approximately 100 and 57 kJ/mol, respectively. This study is a first step in showing the feasibility of using nanoparticles for asphaltene adsorption, followed by catalytic oxidation for heavy oil upgrading.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame machine prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. The Gemma side is a direct model label for every work in the frame, read from the title-only record. The Codex side is a classifier learned from the 10,348 direct Codex labels and calibrated to design-weighted sample rates; fields without enough sample support carry no Codex call. Candidate is the union of the two sides; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: metacan-v3-hybrid-931329e0061cValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.001
Threshold uncertainty score0.002

Distilled classifier scores by category (both heads)

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.022
GPT teacher head0.230
Teacher spread0.208 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one source (direct Gemma or distilled Codex), not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations311
Published2011
Admission routes1
Has abstractyes

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