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Record W2327700868 · doi:10.1021/acssuschemeng.5b00110

Sustainable Catalysts from Gold-Loaded Polyamidoamine Dendrimer-Cellulose Nanocrystals

2015· article· en· W2327700868 on OpenAlex

Why this work is in the frame

A frame that forgets how it found something cannot be audited. These are the routes that admitted this work.

affAt least one author lists a Canadian institution in the pinned OpenAlex snapshot.
fundA Canadian funder is recorded on the work.

Bibliographic record

VenueACS Sustainable Chemistry & Engineering · 2015
Typearticle
Languageen
FieldChemistry
TopicNanomaterials for catalytic reactions
Canadian institutionsCelluForce (Canada)University of Waterloo
FundersNatural Sciences and Engineering Research Council of CanadaCanada Foundation for Innovation
KeywordsDendrimerNanoreactorColloidal goldNanoparticleCatalysisReducing agentDispersityMaterials scienceNanotechnologyChemical engineeringNanochemistryCellulosePotentiometric titrationChemistryPolymer chemistryOrganic chemistry

Abstract

fetched live from OpenAlex

Generation 6.0 polyamidoamine (G6 PAMAM) dendrimer-grafted cellulose nanocrystals (CNCs) (CNC–PAMAM) were synthesized and employed as supports for gold nanoparticles. The successful grafting of PAMAM dendrimers was confirmed by conductometric–potentiometric titration and pH-dependent ζ-potential analyses. Gold nanoparticles with diameters of approximately 2 to 4 nm were synthesized with the PAMAM dendrimers playing the role of nanoreactors and NaBH 4 as the reducing agent. More importantly, gold nanoparticles were successfully prepared at pH 3.3 with the PAMAM dendrimers playing the functional role of reducing agent. Temperature and the concentration of CNC–PAMAM had an impact on the resulting size of gold nanoparticles. The gold nanoparticles immobilized on CNC–PAMAM displayed superior catalytic properties toward the reduction of 4-nitrophenol to 4-aminophenol. The enhanced catalytic behavior may be attributed to the improved dispersity and accessibility of gold nanoparticles within the PAMAM dendrimer domain. This work has demonstrated the versatility of CNC–PAMAM, both as an effective nanoreactor and a reducing agent.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.001
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesMeta-epidemiology (narrow)
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.143
Threshold uncertainty score0.999

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.001
Meta-epidemiology (narrow)0.0010.001
Meta-epidemiology (broad)0.0010.000
Bibliometrics0.0000.001
Science and technology studies0.0000.000
Scholarly communication0.0000.001
Open science0.0010.001
Research integrity0.0010.000
Insufficient payload (model declined to judge)0.0010.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.009
GPT teacher head0.206
Teacher spread0.198 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it