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Record W2328397490 · doi:10.1021/ja211459p

Study of Nucleation and Growth Mechanism of the Metallic Nanodumbbells

2012· article· en· W2328397490 on OpenAlexfundno aff
Galyna Krylova, Lisandro J. Giovanetti, Félix G. Requejo, Nada M. Dimitrijević, Alesia V. Prakapenka, Elena V. Shevchenko

Bibliographic record

VenueJournal of the American Chemical Society · 2012
Typearticle
Languageen
FieldMaterials Science
TopicGold and Silver Nanoparticles Synthesis and Applications
Canadian institutionsnot available
FundersBasic Energy SciencesNatural Sciences and Engineering Research Council of CanadaUniversity of Illinois at ChicagoLaboratório Nacional de Luz SíncrotronOffice of ScienceUniversity of Illinois at Urbana-ChampaignConselho Nacional de Desenvolvimento Científico e TecnológicoConsejo Nacional de Investigaciones Científicas y TécnicasU.S. Department of EnergyNational Science Foundation
KeywordsNucleationChemistryIonNanocrystalMetalGold alloysCrystallographyChemical physicsChemical engineeringPhysical chemistryNanotechnologyMaterials scienceOrganic chemistry

Abstract

fetched live from OpenAlex

We propose a general nucleation and growth model that can explain the mechanism of the formation of CoPt(3)/Au, FePt/Au, and Pt/Au nanodumbbells. Thus, we found that the nucleation event occurs as a result of reduction of Au(+) ions by partially oxidized surface Pt atoms. In cases when Au(3+) is used as a gold precursor, the surface of seeds should be terminated by ions (e.g., Co(2+), Pb(2+)) that can reduce Au(3+) to Au(+) ions, which can further participate in the nucleation of gold domain. Further growth of gold domain is a result of reduction of both Au(3+) and Au(+) by HDA at the surface of gold nuclei. We explain the different ability of CoPt(3), Pt, and FePt seeds to serve as a nucleation center for the reduction of gold and further growth of dumbbells. We report that the efficiency and reproducibility of the formation of CoPt(3)/Au, FePt/Au, and Pt/Au dumbbells can be optimized by the concentration and oxidation states of the surface ions on metallic nanocrystals used as seeds as well as by the type of the gold precursor.

Fetched live from OpenAlex and de-inverted. Abstracts are not stored in this database: the inverted indexes are 8.6 GB of the frame’s 9.3 GB of text, and the host has 13 GB free.

How this classification was reachedexpand

Full frame distilled prediction

Teacher imitation

Not calibrated prevalence, not ground truth. Human validation pending. Learned from the 10,348 direct Codex labels and 10,348 direct Gemma labels. Candidate is the union of thresholded teacher heads; consensus is their intersection. These outputs are machine_predicted_unvalidated and are not human labels or direct frontier model labels.

metaresearch head score (Codex)0.000
metaresearch head score (Gemma)0.000
Version: codex-gemma-dda1882f352aValidation status: machine_predicted_unvalidated
Candidate categoriesnone
Consensus categoriesnone
DomainCandidate signal: none · Consensus signal: none
Study designCandidate signal: Bench or experimental · Consensus signal: Bench or experimental
GenreCandidate signal: Empirical · Consensus signal: Empirical
Teacher disagreement score0.008
Threshold uncertainty score0.107

Codex and Gemma teacher scores by category

CategoryCodexGemma
Metaresearch0.0000.000
Meta-epidemiology (narrow)0.0000.000
Meta-epidemiology (broad)0.0000.000
Bibliometrics0.0000.000
Science and technology studies0.0000.000
Scholarly communication0.0000.000
Open science0.0000.000
Research integrity0.0000.000
Insufficient payload (model declined to judge)0.0000.000

Machine scores (provisional)

The two teacher heads of the student model, read on this work. A score orders the frame for review; it never asserts a category, and the validation status ships verbatim with every row.

Baseline scores from an immature model (maturity gate not passed, 7 training rounds). Scores rank; they never assert a category.

Opus teacher head0.015
GPT teacher head0.240
Teacher spread0.225 · how far apart the two teachers sit on this one work
Validation statusscore_only:v0-immature-baseline · verbatim from the scoring run: score_only means the number may rank works, and no category label ships from it

Classification

machine, unvalidated

Machine predicted; a candidate call from one teacher head, not a consensus.

The models applied no category: nothing in the taxonomy fit this work.
Study designBench or experimental
Domainnot available
GenreEmpirical

How this classification was reached, model by model and score by score, is at the end of the page under "How this classification was reached".

Quick stats

Citations66
Published2012
Admission routes1
Has abstractyes

Explore more

Same venueJournal of the American Chemical SocietySame topicGold and Silver Nanoparticles Synthesis and ApplicationsFrench-language works237,207